1,2-二氯四甲基二硅烷合成路线 （共 115 条）
反应条件
(i) Mg, Et2O, (ii) /BRN= 1736173/, (iii) LiAlH4; Multistep reaction;
参考文献
Cartledge,F.K.; Riedel,K.H.
Journal of Organometallic Chemistry, 1972 , vol. 34, p. 11 - 15
反应条件
(i) Mg, Et2O, (ii) /BRN= 1736173/, (iii) LiAlH4; Multistep reaction;
参考文献
Cartledge,F.K.; Riedel,K.H.
Journal of Organometallic Chemistry, 1972 , vol. 34, p. 11 - 15
反应条件
2-methyl-1H-imidazole; tetra-n-butyl phosphonium chloride T=172 - 177°C; P=5155.93 Torr; 1 h; Autoclave;
参考文献
MOMENTIVE PERFORMANCE MATERIALS INC.; LEWIS, Kenrick, M.; NEELY, John, D.
Patent: WO2013/101619 A1, 2013 ;
Location in patent: Paragraph 0092; 0095 ;
反应条件
hydrogenchloride T=430 - 750°C; 72 h; Conversion of starting material;
参考文献
US2005/113591 A1, ;
Page/Page column 2 ;
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine T=140°C; 20 h;
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5886 - 5893
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine T=145°C; 15 h;
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5886 - 5893
反应条件
water in diethyl ether; acetone 2 h;
参考文献
Chernyavskii; Pleshkova
Russian Chemical Bulletin, 2006 , vol. 55, # 4 p. 748 - 750
反应条件
pyridine; nickel dihydroxide in toluene; acetonitrile Heating;
参考文献
Levitskii; Zavin; Karpilovskaya; Chernyavskii
Russian Chemical Bulletin, 1998 , vol. 47, # 8 p. 1614 - 1616
反应条件
hydrogen sulfide; water; triethylamine in hexane 1 h;
参考文献
Herzog; Rheinwald
Journal of Organometallic Chemistry, 2001 , vol. 627, # 1 p. 23 - 36
反应条件
1: 1,2-dichloro-1,1,2,2-tetramethyldisilane With pyridine in diethyl ether; water; acetone 1 h; cooling; 2: chloro-trimethyl-silane With triethylamine in diethyl ether; water; acetone 1.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Chernyavskii; Pleshkova
Russian Chemical Bulletin, 2006 , vol. 55, # 4 p. 748 - 750
