1,2-二氯四甲基二硅烷合成路线 （共 115 条）
参考文献
Barton, Thomas J.; Jacobi, Stephanie A.
Journal of the American Chemical Society, 1980 , vol. 102, # 27 p. 7979 - 7981
反应条件
1: 3-chloroprop-1-ene With magnesium in diethyl ether
2: 1,2-dichloro-1,1,2,2-tetramethyldisilane in diethyl ether
10 h; Heating;
参考文献
Larkin; Pleshkova; Kononova; Chernyavskaya; Chernyavskii
Russian Chemical Bulletin, 2004 , vol. 53, # 10 p. 2224 - 2228
反应条件
triethylamine in toluene
byproducts: (CH3CH2)3NHCl; (Ar); passing a stream of H2S through a soln. of silicon and tin compds.in toluene with addn. of amine, stirring for 1 h; filtration, evapn.; mass spectrometry;
参考文献
Herzog; Rheinwald
Journal of Organometallic Chemistry, 2001 , vol. 627, # 1 p. 23 - 36
反应条件
1-methyl-1H-imidazole in toluene
3 h; Heating; Product distribution;
参考文献
Herzog; Richter; Brendler; Roewer
Journal of Organometallic Chemistry, 1996 , vol. 507, # 1-2 p. 221 - 228
反应条件
1) hydrolysis, Et2O; 2) pyridine; Yield given. Multistep reaction;
参考文献
Razuaev, G. A.; Brevnova, T. N.; Semenov, V. V.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 8 p. 1806 - 1811,1472 - 1476
反应条件
in diethyl ether; benzene
T=20°C; Rate constantMechanism;
参考文献
Semenov, V. V.; Brevnova, T. N.; Khorshev, S. Ya.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 9 p. 2085 - 2091,1881 - 1887
反应条件
n-butyllithium
1.) ether, 0 deg C, 1 h, 2.) ether, room temperature, 8 h; Yield given. Multistep reaction;
参考文献
Traven', V. F.; Redchenko, V. V.; Eismont, M. Yu.; Stepanov, B. I.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 6 p. 1297 - 1304,1099 - 1105
反应条件
(i) Na-K, (ii) NH4F*HF; Multistep reaction;
参考文献
Kumada,M. et al.
Journal of Organometallic Chemistry, 1966 , vol. 5, p. 120 - 123
反应条件
1-methyl-1H-imidazole in toluene
3 h; Heating; Product distribution;
参考文献
Herzog; Richter; Brendler; Roewer
Journal of Organometallic Chemistry, 1996 , vol. 507, # 1-2 p. 221 - 228
参考文献
Kumada,M. et al.
Journal of Organometallic Chemistry, 1966 , vol. 5, p. 120 - 123
