1,2-二氯四甲基二硅烷合成路线 （共 115 条）
反应条件
bis(benzonitrile)palladium(II) dichloride; triphenylphosphine
T=140°C; 20 h;
参考文献
Rich, Jonathan D.
Journal of the American Chemical Society, 1989 , vol. 111, # 15 p. 5886 - 5893
反应条件
tri-n-butyl-tin hydride; benzildianil in toluene
参考文献
Herzog; Roewer; Ziemer; Herrschaft
Journal of Organometallic Chemistry, 1997 , vol. 533, # 1-2 p. 73 - 77
反应条件
in tetrahydrofuran
T=55 - 60°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Kloster-Jensen, Else; Eliassen, Gudveig Aamdal
Angewandte Chemie, 1985 , vol. 97, # 7 p. 587 - 588
反应条件
ethylmagnesium bromide
1.) THF, 2.) THF, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Iwahara, Takashisa; West, Robert
Journal of the Chemical Society, Chemical Communications, 1988 , # 14 p. 954 - 955
反应条件
magnesium
Grignard reaction; 0.5 h; Reflux;
参考文献
Kai, Hiroyuki; Ohshita, Joji; Ohara, Sayaka; Nakayama, Naohiro; Kunai, Atsutaka; Lee, In-Sook; Kwak, Young-Woo
Journal of Organometallic Chemistry, 2008 , vol. 693, # 23 p. 3490 - 3494
反应条件
in diethyl ether; benzene
T=80°C; 120 h;
参考文献
Brevnova, T. N.; Semenov, V. V.; Razuvaev, G. A.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 9 p. 2010 - 2016,1729 - 1735
反应条件
in diethyl ether; benzene
T=80°C; 120 h;
参考文献
Brevnova, T. N.; Semenov, V. V.; Razuvaev, G. A.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 9 p. 2010 - 2016,1729 - 1735
反应条件
in tetrahydrofuran
T=20 - 50°C; 25 h;
参考文献
Umemiya, Takeshi; Takeuchi, Daisuke; Osakada, Kohtaro
Journal of Organometallic Chemistry, 2006 , vol. 691, # 24-25 p. 5260 - 5266
参考文献
Ando, Wataru; Sugiyama, Mitsuru; Suzuki, Tomohisa; Kato, Chikako; Arakawa, Yusuke; Kabe, Yoshio
Journal of Organometallic Chemistry, 1995 , vol. 499, # 1.2 p. 99 - 112
反应条件
in 1,3,5-trimethyl-benzene
T=165°C;
参考文献
Krafft, Terry E.; Rich, Jonathan D.; McDermott, Philip J.
Journal of Organic Chemistry, 1990 , vol. 55, # 20 p. 5430 - 5432
