萘并[2,1-b]呋喃-2(1H)-酮合成路线 （共 16 条）
反应条件
hydrogenchloride in chloroform T=50°C; 1 h;
参考文献
Kito, Taketoshi; Yoshinaga, Kohji; Yamaya, Makoto; Mizobe, Hoyou
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3336 - 3339
反应条件
triethylamine in tetrahydrofuran T=60°C; 7 h; Yield given;
参考文献
Wilson, R. Marshall; Chantarasiri, Nuanphun
Journal of the American Chemical Society, 1991 , vol. 113, # 6 p. 2301 - 2302
反应条件
potassium hydroxide in water T=30°C; 4.5 h;
参考文献
Marelli, Chiara; Monti, Chiara; Galli, Simona; Masciocchi, Norberto; Piarulli, Umberto
Tetrahedron, 2006 , vol. 62, # 38 p. 8943 - 8951
反应条件
hydrogenchloride in tetrahydrofuran; water T=30°C; 3 h; multistep; Product distribution;
参考文献
Kito, Taketoshi; Yoshinaga, Kohji; Yamaya, Makoto; Mizobe, Hoyou
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3336 - 3339
反应条件
1: 98 percent / aq. KOH / H2O / 3 h / 30 °C 2: 92 percent / 3N aq. HCl / CHCl3 / 1 h / 50 °C View Scheme
参考文献
Kito, Taketoshi; Yoshinaga, Kohji; Yamaya, Makoto; Mizobe, Hoyou
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3336 - 3339
反应条件
1: 78 percent / n-BuLi / tetrahydrofuran / -78 °C 2: 79 percent / 1.) LDA; 2.) aq. satd. NH4Cl / tetrahydrofuran / 6.5 h / -78 - 0 °C 3: 85 percent / HOAc / 20 h / Heating View Scheme
参考文献
Kalinin; Miah; Chattopadhyay; Tsukazaki; Wicki; Nguen; Coelho; Kerr; Snieckus
Synlett, 1997 , vol. 1997, # 7 p. 839 - 841
反应条件
1: 79 percent / 1.) LDA; 2.) aq. satd. NH4Cl / tetrahydrofuran / 6.5 h / -78 - 0 °C 2: 85 percent / HOAc / 20 h / Heating View Scheme
参考文献
Kalinin; Miah; Chattopadhyay; Tsukazaki; Wicki; Nguen; Coelho; Kerr; Snieckus
Synlett, 1997 , vol. 1997, # 7 p. 839 - 841
反应条件
durch Destillation unter vermindertem Druck;
参考文献
Terent'ew et al.
Sb. Statei Obshch. Khim., 1953 , p. 610,613
Chem.Abstr., 1955 , p. 986
参考文献
Ogata et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 1588,1590
反应条件
sulfuric acid T=16 - 18°C; 7 h;
参考文献
Yamaye, Makoto; Motoyanagi, Yoshiko; Nakagawa, Aya; Kametani, Sanae; Yoshinaga, Tetsutaro; Cho, Namiko; Fan, Xiaobo; Kito, Taketoshi
Synthetic Communications, 2004 , vol. 34, # 23 p. 4313 - 4323
