萘并[2,1-b]呋喃-2(1H)-酮合成路线 (共 16 条)
反应条件
2: aqueous hydriodic acid View Scheme
参考文献
Ogata et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 1588,1590
反应条件
1: sodium hydroxide / dimethyl sulfoxide / 2 h / 20 °C 2: n-butyllithium / diethyl ether / 4 h / -78 - -40 °C / |Schlenk technique; |Inert atmosphere 3: 2,6-dimethylpyridine N-oxide; borate(1-), tetrafluoro-,hydrogen (1:1) ethane, 1,1'-oxybis- / 1,4-dioxane / 5 h / 80 °C View Scheme
参考文献
Graf, Katharina; Ruehl, Carmen L.; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12727 - 12731
Angew. Chem., 2013 , vol. 125, # 48 p. 12960 - 12964,5
反应条件
air in water 7 h; Ambient temperatureIrradiationalso under argon atmoshere; photodegradation pathways; Product distribution;
参考文献
Climent, Maria Jose; Miranda, Miguel A.
Journal of Agricultural and Food Chemistry, 1997 , vol. 45, # 5 p. 1916 - 1919
反应条件
1: hydriodic acid; glacial acetic acid 2: durch Destillation View Scheme
参考文献
Mayer; Schaefer; Rosenbach
Archiv der Pharmazie (Weinheim, Germany), 1929 , p. 578
参考文献
I.G. Farbenind.
Patent: DE562391 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 779
Full Text Show Details
Gen. Aniline Works
Patent: US1951686 , 1930 ;
反应条件
sodium hydroxide in methanol 3 h; Heating;
参考文献
Kito, Taketoshi; Yoshinaga, Kohji; Yamaya, Makoto; Mizobe, Hoyou
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3336 - 3339