2-丙基-4-甲基-1,3-二氧噁烷合成路线 （共 6 条）
反应条件
hydrogen; 5 palladium on charcoal in Propylene glycol T=150°C; P=51680.2 Torr; 1 h; Autoclave; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: US2012/330069 A1, 2012 ;
Location in patent: Page/Page column 9-10 ;
反应条件
1: diethyl ether 2: SOCl2, Py View Scheme
参考文献
Trofimov,B.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 2596 - 2600
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 2727 - 2733
反应条件
hydrogen; 5 palladium on charcoal in Propylene glycol T=150°C; P=51680.2 Torr; 1 h; Autoclave; Product distribution / selectivity;
参考文献
EASTMAN CHEMICAL COMPANY
Patent: US2012/330069 A1, 2012 ;
Location in patent: Page/Page column 9-10 ;
反应条件
salicylic acid resin supported FeCl3 in benzene
T=80 - 93°C; 1.8 h;
参考文献
Huirong, Yang; Yingde, Li Bina Cui
Synthetic Communications, 1998 , vol. 28, # 7 p. 1233 - 1238
反应条件
phosphoric acid; hydrogen in water
T=200°C; P=52476.2 Torr; pH=5; 2 h; AutoclaveInert atmosphere; Product distribution / selectivity;
参考文献
DOW GLOBAL TECHNOLOGIES LLC; DESHPANDE, Raj; PANDEY, Vandana; DAVIS, Paul; KORE, Nitin
Patent: WO2011/104719 A1, 2011 ;
Location in patent: Page/Page column 21; 24 ;
反应条件
hydrogen; palladium 10 on activated carbon
T=180°C; P=51716.2 Torr; 3 h; Inert atmosphere;
参考文献
Tulchinsky, Michael L.; Briggs, John R.; Rand, Cynthia L.
Patent: US2010/48940 A1, 2010 ;
Location in patent: Page/Page column 7-8 ;
