反应条件
1: 2-Bromo-N,N-dimethylaniline With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 0°C; 0.75 h; Inert atmosphereSchlenk technique;
2: chloro-diphenylphosphine in tetrahydrofuran; hexane
T=-78 - 0°C; Inert atmosphereSchlenk technique;
参考文献
Richard, Vincent; Ipouck, Melinda; Merel, Delphine S.; Gaillard, Sylvain; Whitby, Richard J.; Witulski, Bernhard; Renaud, Jean-Luc
Chemical Communications, 2014 , vol. 50, # 5 p. 593 - 595