2,2-二苯基-1,3-二氧杂环戊烷合成路线 (共 13 条)
反应条件
hydrogenchloride in 1,4-dioxane; water T=30°C; ΔH(excit.), ΔS(excit)., var. temp.; Rate constantThermodynamic dataKinetics;
参考文献
Ueno, Shinya; Oshima, Takumi; Nagai, Toshikazu
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2131 - 2134
反应条件
lithium in tetrahydrofuran
参考文献
Kaiser,E.M. et al.
Journal of Organic Chemistry, 1971 , vol. 36, # 2 p. 330 - 335
反应条件
pyridine; titanium(III) chloride; lithium in tetrahydrofuran Ring cleavage; McMurry reaction; 16 h; Heating;
参考文献
Synthetic Communications, , vol. 28, # 13 p. 2325 - 2335
反应条件
triethylsilane; palladium dichloride in ethanol 1 h; Inert atmosphereReflux;
参考文献
Journal of the Iranian Chemical Society, , vol. 8, # 2 p. 570 - 573
反应条件
in benzene Ring cleavage; alkylation; 6 h; Heating;
参考文献
Hsieh, Yu-Tsai; Luh, Tien-Yau
Heterocycles, 2000 , vol. 52, # 3 p. 1125 - 1131
反应条件
polyaniline-sulfate salt in toluene
4 h; Heating;
参考文献
Palaniappan, Srinivasan; Narender, Puli; Saravanan, Chandrasekaran; Rao, Vaidya Jayathirtha
Synlett, 2003 , # 12 p. 1793 - 1796
反应条件
DDQ (2,3-dichloro-5,6-dicyano-1,4-benzoquinone) in 1,2-dichloro-ethane
T=20 - 25°C; 2 h;
参考文献
Ueno, Shinya; Oshima, Takumi; Nagai, Toshikazu
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4060 - 4063
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,2-dichloro-ethane
T=20°C; 1 h;
参考文献
Oshima, Takumi; Nishioka, Ryoji; Nagai, Toshikazu
Tetrahedron Letters, 1980 , vol. 21, p. 3919 - 3922
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=-60°C; 1.5 h;
参考文献
Barbasiewicz, Michal; Makosza, Mieczyslaw
Organic Letters, 2006 , vol. 8, # 17 p. 3745 - 3748
反应条件
Montmorillonite clay KSF
T=120°C; 0.5 h; Irradiation;
参考文献
Perio, Bertrand; Dozias, Marie-Joelle; Jacquault, Patrick; Hamelin, Jack
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7867 - 7870