2-苯乙基-1,3-二氧戊环合成路线 （共 21 条）
反应条件
Dess-Martin periodane in dichloromethane; acetonitrile
T=20°C; 12 h;
参考文献
Langille, Neil F; Dakin, Les A; Panek, James S
Organic letters, 2003 , vol. 5, # 4 p. 575 - 578
反应条件
1,3-bis-(diphenylphosphino)propane; cobalt(II) chloride in tetrahydrofuran
T=-15°C; 0.5 h;
参考文献
Ohmiya, Hirohisa; Wakabayashi, Katsuyu; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 10 p. 2207 - 2213
反应条件
[2,2']bipyridinyl; [NiCl2(py)4] in tetrahydrofuran
T=20°C; Negishi coupling reaction; 9 h; Inert atmosphere;
参考文献
Phapale, Vilas B.; Guisan-Ceinos, Manuel; Bunuel, Elena; Cardenas, Diego J.
Chemistry - A European Journal, 2009 , vol. 15, # 46 p. 12681 - 12688
反应条件
Montmorillonite clay KSF
T=80°C; 0.166667 h; Irradiation;
参考文献
Perio, Bertrand; Dozias, Marie-Joelle; Jacquault, Patrick; Hamelin, Jack
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7867 - 7870
反应条件
boron trifluoride diethyl etherate in dichloromethane
1 h; Ambient temperature;
参考文献
Torok, Daniel S.; Figueroa, John J.; Scott, William J.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7274 - 7276
参考文献
Abbott Laboratories
Patent: US5142056 A1, 1992 ;
US 5142056 A
反应条件
N,N,N',N,-tetramethylethylenediamine; C34H46Cl4N10Ni2O2 in tetrahydrofuran
T=20°C; 1.33333 h; Inert atmosphereSchlenk technique;
参考文献
Xue, Fei; Zhao, Jin; Hor, T. S. Andy
Dalton Transactions, 2013 , vol. 42, # 14 p. 5150 - 5158
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; hydrogen; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene
T=110°C; P=22502.3 Torr; 1.5 h; Autoclave; regioselective reaction;
参考文献
Diebolt, Olivier; Cruzeuil, Clement; Mueller, Christian; Vogt, Dieter
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 670 - 677
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; hydrogen; triphenylphosphine
T=110°C; P=22502.3 Torr; 1.5 h; Autoclave; regioselective reaction;
参考文献
Diebolt, Olivier; Cruzeuil, Clement; Mueller, Christian; Vogt, Dieter
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 670 - 677
反应条件
tin(II) trifluoromethanesulfonate; dimethyl tert-butyl silane in acetonitrile
T=0°C;
参考文献
Suzuki, Takeshi; Oriyama, Takeshi
Synthetic Communications, 1999 , vol. 29, # 8 p. 1263 - 1269
