(1-呋喃-2-基-2-苯基乙基)-(4-甲氧基苯基)-胺合成路线 （共 4 条）
反应条件
1: furfural; 4-methoxy-aniline in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
2: benzyl bromide With zinc in tetrahydrofuran
T=20°C; 24 h; Inert atmosphere;
参考文献
Oikawa, Masato; Ikoma, Minoru; Sasaki, Makoto; Gill, Martin B.; Swanson, Geoffrey T.; Shimamoto, Keiko; Sakai, Ryuichi
European Journal of Organic Chemistry, 2009 , # 32 p. 5531 - 5548
反应条件
boron trifluoride diethyl etherate in chloroform
T=50°C; 48 h; Inert atmosphere;
参考文献
Li, Guangxun; Chen, Rong; Wu, Lei; Fu, Qingquan; Zhang, Xiaomei; Tang, Zhuo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 32 p. 8432 - 8436
反应条件
trichlorosilane; N,N-dimethyl-formamide in dichloromethane
T=-10°C;
参考文献
Zheng, Yongsheng; Xue, Zhouyang; Liu, Lixin; Shu, Chang; Yuan, Weicheng; Zhang, Xiaomei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 3 p. 412 - 415
反应条件
1.1: triethylamine; titanium tetrachloride / dichloromethane / 0.5 h / |Inert atmosphere; |Cooling with ice
1.2: 5 h / 20 - 40 °C / |Inert atmosphere
2.1: trichlorosilane; N,N-dimethyl-formamide / dichloromethane / -10 °C
View Scheme
参考文献
Zheng, Yongsheng; Xue, Zhouyang; Liu, Lixin; Shu, Chang; Yuan, Weicheng; Zhang, Xiaomei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 3 p. 412 - 415
