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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
436146-73-5
合成路线
（共 7 条）
→
反应条件
436146-73-5
反应条件
1: in tetrahydrofuran T=20°C; 4 h; 2: With potassium hydroxide in methanol T=20°C; 0.5 h;
参考文献
Miki, Koji; Yokoi, Tomomi; Nishino, Fumiaki; Ohe, Kouichi; Uemura, Sakae
Journal of Organometalic Chemistry, 2002 , vol. 645, # 1-2 p. 228 - 234
234111-16-1
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反应条件
436146-73-5
反应条件
1.1: magnesium / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 1.2: 1 h / -78 - 20 °C / Inert atmosphere 2.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 3.1: potassium fluoride / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Murata, Takahiko; Murai, Masahito; Ikeda, Yuji; Miki, Koji; Ohe, Kouichi
Organic Letters, 2012 , vol. 14, # 9 p. 2296 - 2299
108-86-1
溴代苯
→
反应条件
436146-73-5
反应条件
1.1: magnesium / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 1.2: 1 h / -78 - 20 °C / Inert atmosphere 2.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 3.1: potassium fluoride / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Murata, Takahiko; Murai, Masahito; Ikeda, Yuji; Miki, Koji; Ohe, Kouichi
Organic Letters, 2012 , vol. 14, # 9 p. 2296 - 2299
100-58-3
溴化苯基镁
→
反应条件
436146-73-5
反应条件
1: tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere 2: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 3: potassium fluoride / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Murata, Takahiko; Murai, Masahito; Ikeda, Yuji; Miki, Koji; Ohe, Kouichi
Organic Letters, 2012 , vol. 14, # 9 p. 2296 - 2299
1373776-05-6
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反应条件
436146-73-5
反应条件
Dess-Martin periodane in dichloromethane T=0°C; Dess-Martin Oxidation; Inert atmosphere;
参考文献
Xia, Ying; Qu, Shuanglin; Xiao, Qing; Wang, Zhi-Xiang; Qu, Peiyuan; Chen, Li; Liu, Zhen; Tian, Leiming; Huang, Zhongxing; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2013 , vol. 135, # 36 p. 13502 - 13511
38127-47-8
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反应条件
436146-73-5
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 36 h / 20 °C / |Inert atmosphere 2: tetrahydrofuran / 0 °C / |Inert atmosphere 3: Dess-Martin periodane / dichloromethane / 0 °C / |Inert atmosphere View Scheme
参考文献
Xia, Ying; Qu, Shuanglin; Xiao, Qing; Wang, Zhi-Xiang; Qu, Peiyuan; Chen, Li; Liu, Zhen; Tian, Leiming; Huang, Zhongxing; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2013 , vol. 135, # 36 p. 13502 - 13511
21403-36-1
→
反应条件
436146-73-5
反应条件
1: tetrahydrofuran / 0 °C / |Inert atmosphere 2: Dess-Martin periodane / dichloromethane / 0 °C / |Inert atmosphere View Scheme
参考文献
Xia, Ying; Qu, Shuanglin; Xiao, Qing; Wang, Zhi-Xiang; Qu, Peiyuan; Chen, Li; Liu, Zhen; Tian, Leiming; Huang, Zhongxing; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2013 , vol. 135, # 36 p. 13502 - 13511
