N-甲基-N-(吡啶-2-基)氨基甲酸叔丁酯合成路线 （共 5 条）
反应条件
trifluoroacetic acid in dichloromethane; water
参考文献
Krein, Douglas M.; Lowary, Todd L.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4965 - 4967
反应条件
sodium hydride in N,N-dimethyl-formamide
T=0 - 20°C; 1.5 h;
参考文献
Krein, Douglas M.; Lowary, Todd L.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4965 - 4967
反应条件
1: 98 percent / 2-methyl-propan-2-ol / 24 h / 25 °C
2: 91 percent / NaH / dimethylformamide / 1.5 h / 0 - 20 °C
View Scheme
参考文献
Krein, Douglas M.; Lowary, Todd L.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4965 - 4967
反应条件
1: 98 percent / 2-methyl-propan-2-ol / 24 h / 25 °C
2: 91 percent / NaH / dimethylformamide / 1.5 h / 0 - 20 °C
View Scheme
参考文献
Krein, Douglas M.; Lowary, Todd L.
Journal of Organic Chemistry, 2002 , vol. 67, # 14 p. 4965 - 4967
反应条件
1: tert-butyl alcohol / |Inert atmosphere
2: sodium hydride / tetrahydrofuran / |Inert atmosphere
View Scheme
参考文献
Shewalkar, Mukesh P.; Rao, Ramakrishna R.; Reddy, Veerbhadra; Darandale, Sunil N.; Shinde, Devanand B.
Letters in Organic Chemistry, 2013 , vol. 10, # 1 p. 60 - 64
