2-(1-苯基乙基)-1,3-二氧戊环合成路线 (共 6 条)
反应条件
toluene-4-sulfonic acid in ethylene glycol; toluene
参考文献
Kao Corporation
Patent: US4978653 A1, 1990 ;
反应条件
aluminum oxide in tetrachloromethane
24 h; Heating;
参考文献
Kamitori, Yasuhiro; Hojo, Masaru; Masuda, Ryoichi; Yoshida, Tatsushi
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4767 - 4770
反应条件
in tetrahydrofuran
masked formylation; Heating;
参考文献
Katritzky, Alan R.; Odens, Herman H.; Voronkov, Michael V.
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1886 - 1888
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; hydrogen; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene
T=110°C; P=22502.3 Torr; 1.5 h; Autoclave; regioselective reaction;
参考文献
Diebolt, Olivier; Cruzeuil, Clement; Mueller, Christian; Vogt, Dieter
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 670 - 677
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; hydrogen; triphenylphosphine
T=110°C; P=22502.3 Torr; 1.5 h; Autoclave; regioselective reaction;
参考文献
Diebolt, Olivier; Cruzeuil, Clement; Mueller, Christian; Vogt, Dieter
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 670 - 677
反应条件
AuCl3-CuCl2
5.7 h; Heating;
参考文献
Zhang, Xin; Corma, Avelino
Chemical Communications, 2007 , # 29 p. 3080 - 3082