1-苄基-1H-1,2,3-噻唑合成路线 （共 26 条）
反应条件
triethylamine in methanol
T=0°C; 1 h;
参考文献
Harada, Katsumasa; Oda, Mizuho; Matsushita, Aklo; Shirai, Masashi
Heterocycles, 1998 , vol. 48, # 4 p. 695 - 702
反应条件
CuSO4‵5H2O; potassium carbonate; sodium L-ascorbate in methanol; water
T=20°C; 24 h;
参考文献
Kumar, A. Sudheer; Ghule, Vikas D.; Subrahmanyam; Sahoo, Akhila K.
Chemistry - A European Journal, 2013 , vol. 19, # 2 p. 509 - 518
反应条件
copper(l) iodide; caesium carbonate; sodium L-ascorbate in dimethylsulfoxide-d6; water
T=30°C; 5 h; regioselective reaction;
参考文献
Kim, Taejung; Song, Jung Ho; Jeong, Kyu Hyuk; Lee, Seokjoon; Ham, Jungyeob
European Journal of Organic Chemistry, 2013 , # 19 p. 3992 - 3996
反应条件
copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium L-ascorbate in N,N-dimethyl-formamide
T=150°C; 14 h; Sealed tubeInert atmosphere;
参考文献
Xu, Mei; Kuang, Chunxiang; Wang, Zhuo; Yang, Qing; Jiang, Yubo
Synthesis, 2011 , # 2 art. no. F18110SS, p. 223 - 228
反应条件
in methanol
T=0°C; 4 h;
参考文献
Harada, Katsumasa; Oda, Mizuho; Matsushita, Aklo; Shirai, Masashi
Heterocycles, 1998 , vol. 48, # 4 p. 695 - 702
反应条件
phosphorus trichoride
1 h; Heating;
参考文献
Begtup, Mikael; Jonsson, Gujion
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 10 p. 724 - 735
反应条件
2: Heating
View Scheme
参考文献
Bock; Dammel; Aygen
Journal of the American Chemical Society, 1983 , vol. 105, # 26 p. 7681 - 7685
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Maier, Guenther; Eckwert, Juergen; Bothur, Axel; Reisenauer, Hans Peter; Schmidt, Christiane
Liebigs Annales, 1996 , # 7 p. 1041 - 1053
反应条件
tetrabutyl ammonium fluoride in acetonitrile
12 h; Heating;
参考文献
Ohta, Shunsaku; Kawasaki, Ikuo; Uemura, Takahiro; Yamashita, Masayuki; Yoshioka, Tomomichi; Yamaguchi, Satoshi
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 7 p. 1140 - 1145
参考文献
Wiley et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 190
Full Text View citing articles Show Details
Curtius; Raschig
Journal fuer Praktische Chemie (Leipzig), 1930 , vol. <2>125, p. 466,485
反应条件
1: 98 percent / sodium sulfite / H2O / 1 h / Heating
2: 86 percent / PCl3 / 1 h / Heating
View Scheme
参考文献
Begtup, Mikael; Jonsson, Gujion
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 10 p. 724 - 735
