反应条件
n-butyllithium in tetrahydrofuran
to N-(2-bromobenzyl)-N-methyl-m-tolylamine in THF at -78°C was added n-BuLi in THf, stirred at -78°C for 1 h, added to THF soln. B(OMe)3 at -78°C under Ar, allowed to warm to room temp.; HCl was added and stirred for 1 h, water was added, aq. phase wasextd. with CH2Cl2, organic layers were combined and dried over MgSO4, solvent was removed in vacuo;
参考文献
Ward, Christopher J.; Patel, Prakash; James, Tony D.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 462 - 470