反应条件
1: NaH / tetrahydrofuran; paraffin / 2 h / Heating
2: 1.) NaH / 1.) THF, mineral oil, 0 deg C, 15 min, 2.) THF, mineral oil, 60 deg C, 2 h
3: 2N aq. KOH / ethanol / Ambient temperature
View Scheme
参考文献
Miyamoto, Kenji; Tsuchiya, Shigeo; Ohta, Hiromichi
Journal of Fluorine Chemistry, 1992 , vol. 59, # 2 p. 225 - 232
