3-(3-甲氧基苯基)吡啶合成路线 （共 28 条）
反应条件
Br(1-)*C18H28N3(1+); sodium t-butanolate T=110°C; 4 h; Inert atmosphere;
参考文献
Chen, Wen-Ching; Hsu, Yu-Chen; Shih, Wei-Chun; Lee, Ching-Yu; Chuang, Wen-Han; Tsai, Yi-Fang; Chen, Peter Ping-Yu; Ong, Tiow-Gan
Chemical Communications, 2012 , vol. 48, # 53 p. 6702 - 6704
反应条件
1 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Terashima, Masanao; Seki, Kohichi; Yoshida, Chihiro; Kanaoka, Yuichi
Heterocycles, 1981 , vol. 15, # 2 p. 1075 - 1078
反应条件
6 h; Irradiation; Title compound not separated from byproducts;
参考文献
Terashima, Masanao; Seki, Kohichi; Yoshida, Chihiro; Kanaoka, Yuichi
Heterocycles, 1981 , vol. 15, # 2 p. 1075 - 1078
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide in methanol P=2844.3 Torr; 3 h;
参考文献
Grayson, Neile A.; Bowen, Wayne D.; Rice, Kenner C.
Heterocycles, 1992 , vol. 34, # 12 p. 2281 - 2292
反应条件
1: acetonitrile / 12 h / 110 °C / Sealed tube
2: Adam's catalyst; hydrogen / methanol / 24 h / 20 °C / 3102.97 Torr
View Scheme
参考文献
Ye, Mengchun; Gao, Guo-Lin; Edmunds, Andrew J. F.; Worthington; Morris, James A.; Yu, Jin-Quan
Journal of the American Chemical Society, 2011 , vol. 133, # 47 p. 19090 - 19093
反应条件
1: 90.7 percent / H2, concd. HCl / PtO2 / methanol / 3 h / 2844.3 Torr
View Scheme
参考文献
Grayson, Neile A.; Bowen, Wayne D.; Rice, Kenner C.
Heterocycles, 1992 , vol. 34, # 12 p. 2281 - 2292
反应条件
1: acetone / 20 h / 100 °C / in high pressure vessel
2: H2 / 5percent PtO2/C / methanol / 24 h / Ambient temperature
3: 75 percent / 48percent HBr / 4 h / 120 °C
View Scheme
参考文献
Thorberg; Gawell; Csoregh; Nilsson
Tetrahedron, 1985 , vol. 41, # 1 p. 129 - 139
反应条件
pyridine; hydrogenchloride
T=200°C; 3 h;
参考文献
Wimalasena, D. Shyamali; Perera, Rohan P.; Heyen, Bruce J.; Balasooriya, Inoka S.; Wimalasena, Kandatege
Journal of Medicinal Chemistry, 2008 , vol. 51, # 4 p. 760 - 768
