3,4-二氰基苯甲酰基氯化物合成路线 （共 3 条）
反应条件
thionyl chloride in chloroform
Heating;
参考文献
He, Jianjun; Benkoe, Gabor; Korodi, Ferenc; Polivka, Tomas; Lomoth, Reiner; Akermark, Bjoern; Sun, Licheng; Hagfeldt, Anders; Sundstroem, Villy
Journal of the American Chemical Society, 2002 , vol. 124, # 17 p. 4922 - 4932
反应条件
1: N,N-dimethyl-formamide / 4 h / 150 °C
2: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / water; acetonitrile / 10 °C
3: thionyl chloride / chloroform / 24 h / Reflux; Inert atmosphere
View Scheme
参考文献
An, Minshi; Kim, Soonwha; Hong, Jong-Dal
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 11 p. 3272 - 3278
反应条件
1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / water; acetonitrile / 10 °C
2: thionyl chloride / chloroform / 24 h / Reflux; Inert atmosphere
View Scheme
参考文献
An, Minshi; Kim, Soonwha; Hong, Jong-Dal
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 11 p. 3272 - 3278
