benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in N,N-dimethyl-formamide
T=100°C; 0.5 h;
参考文献
Kumar, Padam Praveen; Reddy, Y. Dathu; Kumari, Y. Bharathi; Devi, B. Rama; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 392 - 398
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in N,N-dimethyl-formamide
T=100°C; 0.5 h;
参考文献
Kumar, Padam Praveen; Reddy, Y. Dathu; Kumari, Y. Bharathi; Devi, B. Rama; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 392 - 398
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in N,N-dimethyl-formamide
T=100°C; 0.5 h;
参考文献
Kumar, Padam Praveen; Reddy, Y. Dathu; Kumari, Y. Bharathi; Devi, B. Rama; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 392 - 398
1: 42 percent / DIEA; PyBOP / dimethylformamide / 24 h / 60 °C
2: 78 percent / aq. NaOH / 1 h / 80 °C
View Scheme
参考文献
Tondi, Donatella; Morandi, Federica; Bonnet, Richard; Costi, M. Paola; Shoichet, Brian K.
Journal of the American Chemical Society, 2005 , vol. 127, # 13 p. 4632 - 4639