2,2',3,3',4,4',5,6,6'-九溴二苯醚合成路线 (共 6 条)
反应条件
bromine; AlCl3, aluminium chloride
T=55 - 61°C; 6.25 h; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION
Patent: WO2008/27776 A2, 2008 ;
Location in patent: Page/Page column 8-9 ;
反应条件
1: With bromine
T=63°C; 1.25 h;
2: With bromine; AlCl3, aluminium chloride
T=59°C; 3.93333 h; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION
Patent: WO2008/27776 A2, 2008 ;
Location in patent: Page/Page column 9-10 ;
反应条件
in methanol; water
1.66667 h; UV-irradiation; KineticsQuantum yield; Further Variations:SolventsReagents;
参考文献
Eriksson, Johan; Green, Nicholas; Marsh, Goeran; Bergman, Ake
Environmental Science and Technology, 2004 , vol. 38, # 11 p. 3119 - 3125
反应条件
bromine; bromine chloride; AlCl3, aluminium chloride
T=55 - 57°C; 2.23333 h; Heating / reflux; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION
Patent: WO2008/27780 A1, 2008 ;
Location in patent: Page/Page column 11-12 ;
反应条件
bromine; bromine chloride; AlCl3, aluminium chloride
T=56°C; 0.0666667 h; Heating / reflux; Product distribution / selectivity;
参考文献
ALBEMARLE CORPORATION
Patent: WO2008/27780 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
honey in acetone
T=60°C; 672 h; Darkness;
参考文献
Wang, Jun; Kliks, Michael M.; Jun, Soojin; Li, Qing X.
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 6 p. 3495 - 3501