4-氨基-3-溴-5-碘苯甲酸乙酯合成路线 （共 3 条）
反应条件
sulfuric acid; sodium nitrite in ethanol; benzene 1.5 h; Heating;
参考文献
Tobe, Yoshito; Utsumi, Naoto; Kawabata, Kazuya; Nagano, Atsushi; Adachi, Kiyomi; Araki, Shunji; Sonoda, Motohiro; Hirose, Keiji; Naemura, Koichiro
Journal of the American Chemical Society, 2002 , vol. 124, # 19 p. 5350 - 5364
反应条件
iodine cloride in water; acetic acid
T=80°C; 10 h;
参考文献
Tobe, Yoshito; Utsumi, Naoto; Kawabata, Kazuya; Nagano, Atsushi; Adachi, Kiyomi; Araki, Shunji; Sonoda, Motohiro; Hirose, Keiji; Naemura, Koichiro
Journal of the American Chemical Society, 2002 , vol. 124, # 19 p. 5350 - 5364
反应条件
1: 99 percent / N-bromosuccinimide / CHCl3 / 4 h / 5 - 10 °C
2: 94 percent / ICl / acetic acid; H2O / 10 h / 80 °C
View Scheme
参考文献
Tobe, Yoshito; Utsumi, Naoto; Kawabata, Kazuya; Nagano, Atsushi; Adachi, Kiyomi; Araki, Shunji; Sonoda, Motohiro; Hirose, Keiji; Naemura, Koichiro
Journal of the American Chemical Society, 2002 , vol. 124, # 19 p. 5350 - 5364
