2,6-二溴-4-甲氧基吡啶1-氧化物合成路线 (共 2 条)
反应条件
phosphorus trichoride in chloroform 0.75 h; Heating;
参考文献
Mongin, Florence; Trecourt, Francois; Gervais, Bruno; Mongin, Olivier; Queguiner, Guy
The Journal of organic chemistry, 2002 , vol. 67, # 10 p. 3272 - 3276
反应条件
1: With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; hexane
T=-75°C; 4 h;
2: With bromocyane in tetrahydrofuran; hexane
T=-75°C; 0.5 h; Further stages.;
参考文献
Mongin, Florence; Trecourt, Francois; Gervais, Bruno; Mongin, Olivier; Queguiner, Guy
The Journal of organic chemistry, 2002 , vol. 67, # 10 p. 3272 - 3276