(3RS,7R,11R)-phytanoyl-CoA; oxygen; iron(II) sulfate Enzyme kinetics; Further Variations:Reagents;

sulfuric acid

sulfuric acid

暂无反应条件数据

thionyl chloride Heating;

toluene-4-sulfonic acid; hydroquinone in ethanol

sulfuric acid 6 h; Reflux;

1: oxalyl chloride / diethyl ether / 1.) 1.25 h, 0 deg C; 2.) 16 h, 25 deg C 2: NaOH / diethyl ether; H2O / 0.75 h / 25 °C / pH = 10.5 - 10.7 3: 63 percent / NBS / dimethylformamide / 20 h / 25 °C 4: 86 percent / 1.) (n-Bu)3SnH; 2.) benzoyl peroxide / CH2Cl2 / 18 h / Heating; Irradiation 5: 67 percent / 48percent HBr / 19.5 h / 100 °C View Scheme

thionyl chloride T=60 - 70°C;