(2-羟基-2,3-二氢-1H-茚-1-基)氨基甲酸叔丁酯合成路线 （共 6 条）
反应条件
hydrogenchloride in methanol; water T=0 - 20°C; Inert atmosphere;
参考文献
Rodriguez-Escrich, Sergi; Sola, Lluis; Jimeno, Ciril; Rodriguez-Escrich, Carles; Pericas, Miquel A.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 14-15 p. 2250 - 2260
反应条件
sodium carbonate in tetrahydrofuran; water
T=0 - 20°C; 3 h;
参考文献
Ren, Qiao; Siau, Woon-Yew; Du, Zhiyun; Zhang, Kun; Wang, Jian
Chemistry - A European Journal, 2011 , vol. 17, # 28 p. 7781 - 7785
反应条件
triethylamine in dichloromethane
T=20°C; 12 h; Title compound not separated from byproducts.;
参考文献
Palmer, Matthew J.; Kenny, Jennifer A.; Walsgrove, Tim; Kawamoto, Aparecida M.; Wills, Martin
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 416 - 427
反应条件
1: Et3N / tetrahydrofuran
2: DEAD; PPh3
3: NaOMe / methanol
View Scheme
参考文献
Qiao, Jennifer X.; Wang, Tammy C.; Wang, Gren Z.; Cheney, Daniel L.; He, Kan; Rendina, Alan R.; Xin, Baomin; Luettgen, Joseph M.; Knabb, Robert M.; Wexler, Ruth R.; Lam, Patrick Y.S.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 18 p. 5041 - 5048
反应条件
1: Et3N / tetrahydrofuran
2: DEAD; PPh3
3: NaOMe / methanol
View Scheme
参考文献
Qiao, Jennifer X.; Wang, Tammy C.; Wang, Gren Z.; Cheney, Daniel L.; He, Kan; Rendina, Alan R.; Xin, Baomin; Luettgen, Joseph M.; Knabb, Robert M.; Wexler, Ruth R.; Lam, Patrick Y.S.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 18 p. 5041 - 5048
反应条件
1: DEAD; PPh3
2: NaOMe / methanol
View Scheme
参考文献
Qiao, Jennifer X.; Wang, Tammy C.; Wang, Gren Z.; Cheney, Daniel L.; He, Kan; Rendina, Alan R.; Xin, Baomin; Luettgen, Joseph M.; Knabb, Robert M.; Wexler, Ruth R.; Lam, Patrick Y.S.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 18 p. 5041 - 5048
