4-[2-(4-氰基苯基)乙基]苯甲腈合成路线 (共 45 条)
反应条件
1: 76 percent / NaBH4 / ethanol / 5 h / Heating
2: 73 percent / 0.03 h / 600 °C / 20 Torr
View Scheme
参考文献
Higuchi, Hiroyuki; Otsubo, Tetsuo; Ogura, Fumio; Yamaguchi, Hachiro; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 1 p. 182 - 187
反应条件
sodium hydride in tetrahydrofuran
3 h; Ambient temperature;
参考文献
Witt, Dariusz; Rachon, Janusz
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 108, # 1-4 p. 169 - 187
反应条件
(i-PrO)2P(O)H; sodium hydride in tetrahydrofuran
3 h; Ambient temperatureIrradiation;
参考文献
Witt, Dariusz; Rachon, Janusz
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 108, # 1-4 p. 169 - 187
反应条件
in dichloromethane
T=0°C; Irradiation; Yield givenYields of byproduct given;
参考文献
Gupta; Dixit, Vandana; Das, Indira
Journal of Organometallic Chemistry, 1999 , vol. 572, # 1 p. 49 - 58
反应条件
phosphorus pentachloride; xylene
参考文献
Sloan; Vaughan
Journal of Organic Chemistry, 1957 , vol. 22, p. 750,759
反应条件
1: concentrated aqueous NH3
2: PCl5; xylene
View Scheme
参考文献
Sloan; Vaughan
Journal of Organic Chemistry, 1957 , vol. 22, p. 750,759
参考文献
Kattwinkel; Wolffenstein
Chemische Berichte, 1901 , vol. 34, p. 2425
Chemische Berichte, 1904 , vol. 37, p. 3221
反应条件
p-benozquinone in hydrogen cyanide
T=190°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Penn, John H.; Deng, Dao-Li
Tetrahedron, 1992 , vol. 48, # 23 p. 4823 - 4830
反应条件
in solid matrix
T=-196°C; Irradiationtemperature dependence of product distributions; Product distribution;
参考文献
Tomioka, Hideo; Suzuki, Shinji; Izawa, Yasuji
Journal of the American Chemical Society, 1982 , vol. 104, # 11 p. 3156 - 3162
反应条件
in acetonitrile
Irradiation;
参考文献
Abe, Manabu; Oku, Akira
Journal of the Chemical Society, Chemical Communications, 1994 , # 14 p. 1673 - 1674