1: benzyl alcohol With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene in dichloromethane 16 h; 2: 1-amino-2-propene With sodium tris(acetoxy)borohydride in dichloromethane chemoselective reaction;
1: With triethylamine in THF-d8 (tetrahydrofuran-d8) T=20°C; 0.0833333 h; Inert atmosphere; 2: With triphenylphosphine in THF-d8 (tetrahydrofuran-d8) T=20°C; Inert atmosphere;
参考文献
Madrahimov, Sherzod T.; Markovic, Dean; Hartwig, John F.
Journal of the American Chemical Society, 2009 , vol. 131, p. 7228 - 7229
1: With hydrogenchloride in diethyl ether T=23°C; 1 h; Inert atmosphere; 2: With sodium hydrogencarbonate in methanol; water T=23°C; 2 h; Inert atmosphere;
参考文献
Cheng, Chen; Brookhart, Maurice
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11304 - 11307
NH4PF6; [Pt(η3-C3H5)(DPP-Xantphos)]PF6 in toluene; acetonitrile T=30°C; 20 h; Inert atmosphere;
参考文献
Mora, Guilhem; Piechaczyk, Olivier; Houdard, Romaric; Mezailles, Nicolas; Le Goff, Xavier-Frederic; Le Floch, Pascal
Chemistry - A European Journal, 2008 , vol. 14, # 32 p. 10047 - 10057
