2-(4-甲氧苯基)-6-甲基吡啶合成路线 （共 9 条）
反应条件
manganese; NiBr2(2,2'-bipyridine); trifluoroacetic acid in N,N-dimethyl-formamide
T=20°C; 4 h;
参考文献
Gosmini, Corinne; Bassene-Ernst, Carine; Durandetti, Muriel
Tetrahedron, 2009 , vol. 65, # 31 p. 6141 - 6146
反应条件
C42H64O4P2Pd in tetrahydrofuran
T=60°C; Kumada-Corriu coupling reaction; 20 h; Inert atmosphere; chemoselective reaction;
参考文献
Ackermann, Lutz; Potukuchi, Harish K.; Kapdi, Anant R.; Schulzke, Carola
Chemistry - A European Journal, 2010 , vol. 16, # 11 p. 3300 - 3303
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane
T=100 - 110°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Zhao, Yu-Long; Li, You; Li, Shui-Ming; Zhou, Yi-Guo; Sun, Feng-Yi; Gao, Lian-Xun; Han, Fu-She
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1543 - 1550
反应条件
C42H64O4P2Pd in tetrahydrofuran
T=60°C; Kumada-Corriu coupling reaction; 20 h; Inert atmosphere; chemoselective reaction;
参考文献
Ackermann, Lutz; Potukuchi, Harish K.; Kapdi, Anant R.; Schulzke, Carola
Chemistry - A European Journal, 2010 , vol. 16, # 11 p. 3300 - 3303
反应条件
in acetic acid
Heating; Yield given. Yields of byproduct given;
参考文献
Petrich; Petrich, Scott A.; Hicks; Hicks, Fred A.; Wilkinson; Wilkinson, Doug R.; Tarrant; Tarrant, James G.; Bruno; Bruno, Steve M.; Vargas; Vargas, Marian; Hosein; Hosein, Kirsten N.; Gupton; Gupton, John T.; Sikorski; Sikorski, James A.
Tetrahedron, 1995 , vol. 51, # 6 p. 1575 - 1584
反应条件
sodium hydride
1.) DMF, 15 min, 2.) DMF, 100 deg C, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Petrich; Petrich, Scott A.; Hicks; Hicks, Fred A.; Wilkinson; Wilkinson, Doug R.; Tarrant; Tarrant, James G.; Bruno; Bruno, Steve M.; Vargas; Vargas, Marian; Hosein; Hosein, Kirsten N.; Gupton; Gupton, John T.; Sikorski; Sikorski, James A.
Tetrahedron, 1995 , vol. 51, # 6 p. 1575 - 1584
反应条件
in acetic acid
Heating; Yield given. Yields of byproduct given;
参考文献
Petrich; Petrich, Scott A.; Hicks; Hicks, Fred A.; Wilkinson; Wilkinson, Doug R.; Tarrant; Tarrant, James G.; Bruno; Bruno, Steve M.; Vargas; Vargas, Marian; Hosein; Hosein, Kirsten N.; Gupton; Gupton, John T.; Sikorski; Sikorski, James A.
Tetrahedron, 1995 , vol. 51, # 6 p. 1575 - 1584
反应条件
in acetic acid
Heating; Yield given. Yields of byproduct given;
参考文献
Petrich; Petrich, Scott A.; Hicks; Hicks, Fred A.; Wilkinson; Wilkinson, Doug R.; Tarrant; Tarrant, James G.; Bruno; Bruno, Steve M.; Vargas; Vargas, Marian; Hosein; Hosein, Kirsten N.; Gupton; Gupton, John T.; Sikorski; Sikorski, James A.
Tetrahedron, 1995 , vol. 51, # 6 p. 1575 - 1584
反应条件
1: 4-methoxy-aniline With tetrafluoroboric acid; sodium nitrite in water
T=0°C; Inert atmosphere;
2: 2-methyl pyridine hydrochloride With [Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in water
T=25°C; 80 h; IrradiationInert atmosphere; Catalytic behavior;
参考文献
Xue, Dong; Jia, Zhi-Hui; Zhao, Cong-Jun; Zhang, Yan-Yan; Wang, Chao; Xiao, Jianliang
Chemistry - A European Journal, 2014 , vol. 20, # 10 p. 2960 - 2965
