4,4'-二甲基-1,1'-联苯-2,2',5,5'-四酮合成路线 (共 7 条)
反应条件
1: With sulfuric acid; acetic anhydride T=20°C; 23 h; 2: With hydrogenchloride; methanol 3: With anhydrous iron chloride in ethanol; water
参考文献
Love, Brian E.; Bonner-Stewart, Jeffrey; Forrest, Lori A.
Tetrahedron Letters, 2009 , vol. 50, # 35 p. 5050 - 5052
反应条件
ammonium cerium (IV) nitrate in water; acetonitrile
T=20°C; 1 h; Solvent;
参考文献
Love, Brian E.; Duffy, Brian C.; Simmons, Alexander L.
Tetrahedron Letters, 2014 , vol. 55, # 12 p. 1994 - 1997
反应条件
cerium ammonium nitrate; silica gel in dichloromethane
参考文献
Ali, Mohammed Hashmat; Niedbalski, Melinda; Bohnert, Gary; Bryant, Daniel
Synthetic Communications, 2006 , vol. 36, # 12 p. 1751 - 1759
反应条件
oxygen; acetic acid; bis(1,3-propanediaminato)copper(II) chloride in ethanol
3 h; Heating;
参考文献
Paraskevas, Spyridon M.; Konstantinidis, Demetrios; Vassilara, Georgia
Synthesis, 1988 , # 11 p. 897 - 899
反应条件
dihydrogen peroxide; iron(II) sulfate
参考文献
Ono; Oyamada
Bulletin of the Chemical Society of Japan, 1936 , vol. 11, p. 132,135, 137
参考文献
Erdtman
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1934 , vol. 143, p. 196,197
Chem. Zentralbl., 1934 , vol. 105, # I p. 3054
反应条件
1: With sulfuric acid; acetic anhydride
T=20°C; 23 h;
2: With hydrogenchloride; methanol
Further stages;
参考文献
Love, Brian E.; Bonner-Stewart, Jeffrey; Forrest, Lori A.
Tetrahedron Letters, 2009 , vol. 50, # 35 p. 5050 - 5052