2-甲基-1,3-二氧戊环-2-丙酸合成路线 (共 13 条)
反应条件
lithium aluminium tetrahydride in diethyl ether
T=0°C; 0.5 h;
参考文献
Joubert; Beney; Marsura; Luu-Duc
Journal of Labelled Compounds and Radiopharmaceuticals, 1995 , vol. 36, # 8 p. 745 - 754
参考文献
Moreau, Jean-Louis; Couffignal, Renee
Journal of Organometallic Chemistry, 1985 , vol. 294, p. 139 - 144
反应条件
1: 85 percent / pyridine / diethyl ether / Heating
2: 84 percent / i-Pr2NLi / diethyl ether / -60 °C
3: 87 percent / H2SO4 / H2O; acetone / 4 h / 40 - 45 °C
View Scheme
参考文献
Moreau, J.-L.; Couffignal, R.; Arous-Chtara, R.
Tetrahedron, 1981 , vol. 37, p. 307 - 310