1-苯基-2-丙烯-1-醇合成路线 （共 252 条）
反应条件
(η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate in tetrahydrofuran; toluene T=40°C; Mannich type reaction; 15 h; Inert atmosphereMolecular sieve; optical yield given as percent dediastereoselective reaction;
参考文献
Bartoszewicz, Agnieszka; Jezowska, Martina M.; Laymand, Kevin; Moebus, Juri; Martin-Matute, Belen
European Journal of Inorganic Chemistry, 2012 , # 9 p. 1517 - 1530
反应条件
(η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate in tetrahydrofuran; toluene T=40°C; Mannich type reaction; 11 h; Inert atmosphereMolecular sieve; optical yield given as percent dediastereoselective reaction;
参考文献
Bartoszewicz, Agnieszka; Jezowska, Martina M.; Laymand, Kevin; Moebus, Juri; Martin-Matute, Belen
European Journal of Inorganic Chemistry, 2012 , # 9 p. 1517 - 1530
反应条件
(η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate; sodium carbonate in tetrahydrofuran; toluene T=35°C; 13 h; Inert atmosphere;
参考文献
Bartoszewicz, Agnieszka; Jezowska, Martina M.; Laymand, Kevin; Moebus, Juri; Martin-Matute, Belen
European Journal of Inorganic Chemistry, 2012 , # 9 p. 1517 - 1530
反应条件
(η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate in tetrahydrofuran; toluene T=40°C; Mannich type reaction; 14 h; Inert atmosphereMolecular sieve; optical yield given as percent dediastereoselective reaction;
参考文献
Bartoszewicz, Agnieszka; Jezowska, Martina M.; Laymand, Kevin; Moebus, Juri; Martin-Matute, Belen
European Journal of Inorganic Chemistry, 2012 , # 9 p. 1517 - 1530
反应条件
[RuCl2(.eta.6-p-cymene)((R)-PhOP(binaphthoxy))]; potassium tert-butylate in tetrahydrofuran T=45°C; 0.25 h; Inert atmosphereResolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Fernandez-Zumel, Mariano A.; Lastra-Barreira, Beatriz; Scheele, Marcus; Diez, Josefina; Crochet, Pascale; Gimeno, Jose
Dalton Transactions, 2010 , vol. 39, # 33 p. 7780 - 7785
反应条件
n-butyllithium; benzyl bromide; [Rh(dppe)(NBD)]ClO4 1.) THF, hexane, 60 deg C, 7 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
反应条件
n-butyllithium; [Rh(dppe)(NBD)]ClO4 1.) THF, hexane, 60 deg C, 7 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
反应条件
n-butyllithium; [Rh(dppe)(NBD)]ClO4 1.) THF, hexane, 60 deg C, 7 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
反应条件
n-butyllithium; [Rh(dppe)(NBD)]ClO4 1.) THF, hexane, 60 deg C, 7 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
反应条件
n-butyllithium; [Rh(dppe)(NBD)]ClO4 1.) THF, hexane, 60 deg C, 7 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
