1-苯基-2-丙烯-1-醇合成路线 （共 252 条）
反应条件
triethylamine in dichloromethane; dimethyl sulfoxide
参考文献
Matsumoto, Takahiro; Katayama, Nozomi; Mabuchi, Hiroshi
Patent: US2003/144338 A1, 2003 ;
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride in 1,2-dichloro-ethane
参考文献
Tetrahedron Letters, , vol. 52, # 25 p. 3208 - 3211
反应条件
n-butyllithium; [Rh(dppe)(NBD)]ClO4 1.) THF, hexane, 60 deg C, 7 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
反应条件
2,9-dimethyl-1,10-phenanthroline; palladium diacetate; copper(l) chloride in dimethyl sulfoxide T=50°C; P=760.051 Torr; 12 h;
参考文献
Vellakkaran, Mari; Andappan, Murugaiah M.S.; Kommu, Nagaiah
Green Chemistry, 2014 , vol. 16, # 5 p. 2788 - 2797
反应条件
triethylamine; palladium diacetate in acetonitrile T=100°C; 24 h;
参考文献
Briot, Anne; Baehr, Corinne; Brouillard, Raymond; Wagner, Alain; Mioskowski, Charles
Journal of Organic Chemistry, 2004 , vol. 69, # 4 p. 1374 - 1377
反应条件
tetrabutylammomium bromide; oxygen; palladium diacetate in water; dimethyl sulfoxide; N,N-dimethyl-formamide T=120°C; Heck Reaction; P=760.051 Torr; Schlenk technique;
参考文献
Huang, Liangbin; Qi, Ji; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemistry - A European Journal, 2013 , vol. 19, # 46 p. 15462 - 15466
反应条件
1: 3-phenyl-3-hydroxypropene With α-cyclohexylcyclohexanemethanamine in water T=20°C; Heck reaction; 0.25 h; 2: iodobenzene With 4'-hydroxyacetophenone oxime palladacycle catalyst in water T=120°C; Heck reaction; 10 h; Further stages.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
反应条件
1: 3-phenyl-3-hydroxypropene With α-cyclohexylcyclohexanemethanamine in water T=20°C; Heck reaction; 0.25 h; 2: iodobenzene With Kaiser oxime-derived complex on resin base in water T=120°C; Heck reaction; 16 h; Further stages. Title compound not separated from byproducts.;
参考文献
Alacid, Emilio; Najera, Carmen
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2572 - 2584
反应条件
1: pyridine 2: hydrogen / toluene / 16 h / 60 °C View Scheme
参考文献
Noujima, Akifumi; Mitsudome, Takato; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Chemical Communications, 2012 , vol. 48, # 53 p. 6723 - 6725
参考文献
Klages
Chemische Berichte, 1906 , vol. 39, p. 2589
