1-苯基-2-丙烯-1-醇合成路线 (共 252 条)
参考文献
Klages
Chemische Berichte, 1906 , vol. 39, p. 2589
参考文献
Klages
Chemische Berichte, 1906 , vol. 39, p. 2589
反应条件
1: MnO2 / ethyl acetate 2: ethyl-5-(2-hydroxyethyl)-4-methylthiazolium bromide, NEt3 / 2 h / 90 °C 3: TsOH / toluene / 100 °C View Scheme
参考文献
Perrier, Helene; Bayly, Christopher; Laliberte, France; Huang, Zheng; Rasori, Roberta; Robichaud, Annette; Girard, Yves; Macdonald, Dwight
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 3 p. 323 - 326
反应条件
1,1'-bis(diphenylphosphino)ferrocene; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; 4-hydroxybutanol; potassium tert-butylate T=110°C; 24 h; Inert atmosphere;
参考文献
Maytum, Hannah C.; Francos, Javier; Whatrup, David J.; Williams, Jonathan M. J.
Chemistry - An Asian Journal, 2010 , vol. 5, # 3 p. 538 - 542
反应条件
triethylamine; palladium on activated charcoal in toluene T=150°C; 3 h;
参考文献
Journal of Organometallic Chemistry, , vol. 692, # 22 p. 4805 - 4808
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride in 1,2-dichloro-ethane
参考文献
Tetrahedron Letters, , vol. 52, # 25 p. 3208 - 3211
反应条件
toluene-4-sulfonic acid; benzyl azide in dichloromethane Schmidt Reaction; 5.5 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 14, # 22 p. 5728 - 5731
反应条件
1: m-chloroperbenzoic acid / CH2Cl2 2: tetra-n-propylammonium perruthenate; N-methyl morpholine oxide / CH2Cl2 / 1 h / 25 °C 3: 93 percent / (tris(1-pyrazolyl)borate)RuPPh3(CH3CN)2PF6 / toluene / 5 h / 100 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 8 p. 2793 - 2796
反应条件
1: MnO2 / ethyl acetate 2: ethyl-5-(2-hydroxyethyl)-4-methylthiazolium bromide, NEt3 / 2 h / 90 °C View Scheme
参考文献
Perrier, Helene; Bayly, Christopher; Laliberte, France; Huang, Zheng; Rasori, Roberta; Robichaud, Annette; Girard, Yves; Macdonald, Dwight
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 3 p. 323 - 326
反应条件
1: With bis(η3-allyl-μ-chloropalladium(II)); N,N-dicyclohexylmethylamine; P(t-Bu)2(2'-methylbiphenyl-2-yl) in acetonitrile T=90°C; Improved Larock synthesis; 0.5 h; Inert atmosphere; 2: With di-isopropyl azodicarboxylate; acetic acid in acetonitrile T=90°C; Improved Larock synthesis; 0.25 h; Inert atmosphere;
参考文献
Stone, Matthew T.
Organic Letters, 2011 , vol. 13, # 9 p. 2326 - 2329