1-苯基-2-丙烯-1-醇合成路线 （共 252 条）
反应条件
sodium hydrogencarbonate; triphenylphosphine; palladium dichloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=140°C; 24 h;
参考文献
Larock, Richard C.; Kuo, Mann-Yan
Tetrahedron Letters, 1991 , vol. 32, # 5 p. 569 - 572
反应条件
triethyl borane; palladium diacetate; triethylamine; triphenylphosphine; lithium chloride in tetrahydrofuran; hexane T=20°C; Tsuji-Trost Allylation; 48 h; Inert atmosphere;
参考文献
Brown, Adam R.; Uyeda, Christopher; Brotherton, Carolyn A.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2013 , vol. 135, # 18 p. 6747 - 6749
反应条件
Pt(COD)Cl2; bis[2-(diphenylphosphino)phenyl] ether in 1,4-dioxane 18 h; Heating;
参考文献
Utsunomiya, Masaru; Miyamoto, Yoshiki; Lpposhi, Junji; Ohshima, Takashi; Mashima, Kazushi
Organic Letters, 2007 , vol. 9, # 17 p. 3371 - 3374
反应条件
acetyl chloride in ethanol T=23°C; 0.25 h;
参考文献
Yadav, Veejendra K.; Ganesh Babu
Tetrahedron, 2003 , vol. 59, # 46 p. 9111 - 9116
反应条件
in dichloromethane T=20°C; 12 h;
参考文献
Kishali, Nurhan; Polat, M. Fatih; Altundas, Ramazan; Kara, Yunus
Helvetica Chimica Acta, 2008 , vol. 91, # 1 p. 67 - 72
反应条件
T=40°C; Einleiten von HCl;
参考文献
Martin; Trinh
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 228, p. 688
参考文献
Rupe; Mueller
Helvetica Chimica Acta, 1921 , vol. 4, p. 847
反应条件
1.1: 76 percent / DMAP; pyridine / CH2Cl2 / 16 h / Heating 2.1: ozone / CH2Cl2; methanol / -78 °C 2.2: 73 percent / Me2S / CH2Cl2; methanol / 3 h / 20 °C 3.1: KHMDS; 18-crown-6 / tetrahydrofuran / 0.5 h / -78 °C 3.2: tetrahydrofuran / 3 h / -78 °C 4.1: O3 / CH2Cl2; methanol 4.2: NaBH4 / propan-2-ol 5.1: KOH / methanol View Scheme
参考文献
Pedersen; Hansen; Kane; Rein; Helquist; Norrby; Tanner
Journal of the American Chemical Society, 2001 , vol. 123, # 40 p. 9738 - 9742
反应条件
1.1: 76 percent / DMAP; pyridine / CH2Cl2 / 16 h / Heating 2.1: ozone / CH2Cl2; methanol / -78 °C 2.2: 73 percent / Me2S / CH2Cl2; methanol / 3 h / 20 °C 3.1: KHMDS; 18-crown-6 / tetrahydrofuran / 0.5 h / -78 °C 3.2: tetrahydrofuran / 3 h / -78 °C 4.1: O3 / CH2Cl2; methanol 4.2: NaBH4 / propan-2-ol 5.1: KOH / methanol View Scheme
参考文献
Pedersen; Hansen; Kane; Rein; Helquist; Norrby; Tanner
Journal of the American Chemical Society, 2001 , vol. 123, # 40 p. 9738 - 9742
反应条件
bismuth trifluoromethanesulphonate in nitromethane T=100°C; 2 h;
参考文献
Organic Letters, , vol. 9, # 5 p. 825 - 828
