1-苯基-2-丙烯-1-醇合成路线 （共 252 条）
反应条件
sodium hydrogencarbonate; palladium diacetate in water
T=60°C; 0.0833333 h; Title compound not separated from byproducts.;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
Synthesis, 2006 , # 20 p. 3443 - 3452
反应条件
(COBr)2; dimethyl sulfoxide; triethylamine in dichloromethane
T=-78 - 20°C; 1.5 h;
参考文献
Yin, Jiandong; Gallis, Christina E.; Chisholm, John D.
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 7054 - 7057
反应条件
1: mercury(II) acetate / Ambient temperature
2: 49 percent Spectr. / methylaluminum bis(4-bromo-2,6-di-tert-butylphenoxide) (reagent A) / CH2Cl2 / 0.25 h / -78 °C
View Scheme
参考文献
Nonshita, Katsumasa; Banno, Hiroshi; Maruoka, Keiji; Yamamoto, Hishashi
Journal of the American Chemical Society, 1990 , vol. 112, # 1 p. 316 - 322
反应条件
tetrabutylammomium bromide; oxygen; palladium diacetate in water; dimethyl sulfoxide; N,N-dimethyl-formamide
T=120°C; Heck Reaction; P=760.051 Torr; Schlenk technique;
参考文献
Huang, Liangbin; Qi, Ji; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemistry - A European Journal, 2013 , vol. 19, # 46 p. 15462 - 15466
反应条件
sodium acetate; palladium diacetate in acetonitrile
T=60°C; 2 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
Synthesis, 2006 , # 20 p. 3443 - 3452
反应条件
sodium hydrogencarbonate; palladium diacetate in water
T=60°C; 0.333333 h; Title compound not separated from byproducts.;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
Synthesis, 2006 , # 20 p. 3443 - 3452
参考文献
Toda, Fumio; Matsuda, Shotaro; Tanaka, Koichi
Tetrahedron: Asymmetry, 1991 , vol. 2, # 10 p. 983 - 986
反应条件
(i) tBuOCl, (ii) benzene-1,4-diol; Multistep reaction;
参考文献
Kartashov,V.R. et al.
Journal of Organic Chemistry USSR (English Translation), 1971 , vol. 7, p. 1634 - 1637
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 8 p. 1574 - 1577
反应条件
n-butyllithium; benzyl bromide; [Rh(dppe)(NBD)]ClO4
1.) THF, hexane, 60 deg C, 7 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
反应条件
n-butyllithium; [Rh(dppe)(NBD)]ClO4
1.) THF, hexane, 60 deg C, 7 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993
