反应条件
titanium(IV) isopropylate; magnesium bromide; (1S,2R,4R,1'R,2'R,1''S,2''R,4''R)-N-{trans-2'-[2''-hydroxy-7'',7''-dimethylbicyclo[2.2.1]hept-1''-ylmethylsulfonamino]cyclohexyl}-2-hydroxy-7,7-dimethylbicyclo[2.2.1]hept-1-ylmethanesulfonamide in toluene
T=0°C; 12 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Chen, Chien-An; Wu, Kuo-Hui; Gau, Han-Mou
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 10 p. 1626 - 1634
