反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1.1: n-BuLi / diethyl ether; hexane / 0.42 h / -40 °C<br />1.2: diethyl ether; hexane / 8 h / Heating<br />2.1: 5.1 g / LiAlH<sub>4</sub> / diethyl ether / Heating<br />3.1: 41 percent / benzene / 4 h / 85 °C<br />4.1: n-BuLi / diethyl ether; hexane / 0.17 h / -78 °C<br />4.2: 56 percent / HBr gas / diethyl ether; hexane / -78 - 20 °C<br /> <br />
参考文献
Allen, John M.; Aprahamian, Steve L.; Sans, Esther A.; Shechter, Harold Journal of Organic Chemistry, 2002 , vol. 67, # 11 p. 3561 - 3574
