in ethanol soln. of organic ligand in ethanol added dropwise with stirring to soln.of NiCl2*6H2O in ethanol; stirred for 4 h at 60 °C then cooled s lowly to room temp.; crystals filtered and washed with cold ethanol and dried on air; elem. anal.;
参考文献
Colak, Alper Tolga; Tas, Murat; Irez, Gazi; Yesilel, Okan Zafer; Bueyuekguengoer, Orhan
Zeitschrift fur Anorganische und Allgemeine Chemie, 2007 , vol. 633, # 3 p. 504 - 508
