N,N-双(乙烯)-对甲苯磺酰胺合成路线 （共 21 条）
反应条件
in water
Decomposition; photodegradation; pH=9; Irradiation; Product distribution; Further Variations:pH-values;
参考文献
Hill, Roger R.; Jeffs, Graham E.; Roberts, David R.; Wood, Sharon A.
Chemical Communications, 1999 , # 17 p. 1735 - 1736
参考文献
Protiva; Borovicka
Chemicke Listy, 1952 , vol. 46, p. 427
Chem.Abstr., 1953 , p. 4300
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Vyas; Dhopate
Journal of Scientific and Industrial Research, 1959 , vol. 18 C, p. 6,9
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Masuda
Kobunshi Kagaku, 1955 , vol. 12, p. 356,360
Chem.Abstr., 1957 , p. 2651
反应条件
sodium ethanolate
1.) ethanol, reflux, 1 h, 2.) DMF, RT, 12 h; Yield given. Multistep reaction;
参考文献
Dale, Johannes; Sigvartsen, Turid
Acta Chemica Scandinavica, 1991 , vol. 45, # 10 p. 1064 - 1070
反应条件
boron trichloride in dichloromethane
T=0 - 20°C;
参考文献
Beckmann, Edith; Hoppe, Dieter
Synthesis, 2005 , # 2 art. no. T09504SS, p. 217 - 222
反应条件
boron tribromide in dichloromethane
T=20°C; 0.5 h;
参考文献
Kiyooka, Syun-Ichi; Fujiyama, Ryoji; Uddin, Md. Khabir; Goh, Kazuki; Nagano, Yoshiya; Fujio, Mizue; Tsuno, Yuho
Tetrahedron Letters, 2005 , vol. 46, # 2 p. 209 - 212
反应条件
sodium in ethanol; N,N-dimethyl-formamide
T=80°C;
参考文献
Iwata, Masaaki; Kuzuhara, Hiroyoshi
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 4 p. 1031 - 1036
反应条件
potassium carbonate in N,N-dimethyl-formamide
53 h; Ambient temperaturealso other reaction conditions; Product distribution;
参考文献
Iwata, Masaaki; Kuzuhara, Hiroyoshi
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 4 p. 1031 - 1036
反应条件
caesium carbonate in N,N-dimethyl-formamide
1) room temperature, 12 h, 2) 60 deg C, 4 h;
参考文献
Craig, Andrew S.; Kataky, Ritu; Matthews, Robert C.; Parker, David; Ferguson, George; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 9 p. 1523 - 1531
反应条件
(i) KOtBu, DMF, (ii) /BRN= 583800/; Multistep reaction;
参考文献
Gunnlaugsson, Thorfinnur; Bichell, Bastien; Nolan, Claire
Tetrahedron, 2004 , vol. 60, # 27 p. 5799 - 5806
反应条件
1: 1,4-bis-(p-toluenesulfonyl)-1,4-diazabutane With lithium hydride in N,N-dimethyl-formamide
T=70°C; 2 h;
2: 4-methyl-N,N-bis[2-[[(4-methylphenyl)sulfonyl]oxy]ethyl]benzenesulfonamide in N,N-dimethyl-formamide
T=50°C; 120 h; Further stages.;
参考文献
Stones, Graham; Tripoli, Regis; McDavid, Colin L.; Roux-Duplgtre, Kewin; Kennedy, Alan R.; Sherrington, David C.; Gibson, Colin L.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 2 p. 374 - 384
