4-氨基-4-甲基-2-戊醇合成路线 （共 23 条）
反应条件
1: With ammonia in methanol T=26°C; 2 h; 2: With sodium tetrahydroborate in methanol 2 h; Reflux;
参考文献
Zubkov, Fedor I.; Nikitina, Eugenia V.; Galeev, Timur R.; Zaytsev, Vladimir P.; Khrustalev, Victor N.; Novikov, Roman A.; Orlova, Daria N.; Varlamov, Alexey V.
Tetrahedron, 2014 , vol. 70, # 8 p. 1659 - 1690
反应条件
sodium hydroxide in water
参考文献
Research Corporation Technologies, Inc.
Patent: US4908356 A1, 1990 ;
反应条件
sodium amalgam; ethanol; ammonia; water
参考文献
Kahan
Chemische Berichte, 1897 , vol. 30, p. 1319
Full Text Show Details
Heintz
Justus Liebigs Annalen der Chemie, 1876 , vol. 183, p. 291
反应条件
water; nickel T=120 - 140°C; P=51485.6 Torr; Hydrogenation;
参考文献
Shell Devel Co.
Patent: US2497548 , 1947 ;
参考文献
Smith; Adkins
Journal of the American Chemical Society, 1938 , vol. 60, p. 407
反应条件
1: Raney nickel; dioxane / 160 - 170 °C / 73550.8 - 147102 Torr / Hydrogenation.bis zur Aufnahme von 1 Mol Wasserstoff 2: NaOH View Scheme
参考文献
Smith; Adkins
Journal of the American Chemical Society, 1938 , vol. 60, p. 407
反应条件
sulfuric acid; acetonitrile in n-heptane T=0°C; 5 h; Title compound not separated from byproducts;
参考文献
Kuznetsov
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 1 p. 127 - 128
反应条件
sulfuric acid in n-heptane T=0°C; 5 h; Title compound not separated from byproducts;
参考文献
Kuznetsov
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 1 p. 127 - 128
反应条件
nickel diacetate in methanol 1 h; Ambient temperature;
参考文献
Yoon; Choi; Shon
Synthetic Communications, 1993 , vol. 23, # 21 p. 3047 - 3053
参考文献
Belly,A. et al.
Bulletin de la Societe Chimique de France, 1972 , p. 330 - 336
