2,2'-亚甲基二[1,3-二氧戊环]合成路线 （共 6 条）
反应条件
hydroxylamine hydrochloride T=110 - 120°C; Green chemistry;
参考文献
Nitlikar, Lakshmikant H.; Shinde, Devanand B.
Letters in Organic Chemistry, 2013 , vol. 10, # 9 p. 637 - 639
反应条件
toluene-4-sulfonic acid in ethylene glycol; toluene
T=110 - 120°C; Green chemistry;
参考文献
Nitlikar, Lakshmikant H.; Shinde, Devanand B.
Letters in Organic Chemistry, 2013 , vol. 10, # 9 p. 637 - 639
反应条件
toluene-4-sulfonic acid in toluene
Heating;
参考文献
Martinez-Bernhardt, Rolando; Castro, Peter P.; Godjoian, Gayane; Gutierrez, Carlos G.
Tetrahedron, 1998 , vol. 54, # 31 p. 8919 - 8932
反应条件
KU-2-8 cation-exchange resin
T=110 - 120°C; heating until alcohol liberation was complete;
参考文献
Imashev, U. B.; Kalashnikov, S. M.; Gordeeva, G. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 4 p. 369 - 373
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , # 4 p. 459 - 463
反应条件
hydrogenchloride in chloroform
36 h; Ambient temperature;
参考文献
Shi-Qi, Peng; Winterfeldt, Ekkehard
Liebigs Annalen der Chemie, 1989 , p. 1045 - 1047
反应条件
pyridine; N,N'-dimethyl-N,N'-propyleneurea; 1,10-phenanthroline; NiI2*3.5H2O; sodium iodide; zinc
T=20 - 60°C; 19 h; chemoselective reaction;
参考文献
Everson, Daniel A.; Jones, Brittany A.; Weix, Daniel J.
Journal of the American Chemical Society, 2012 , vol. 134, # 14 p. 6146 - 6159
