2-甲基-N-苯基丙酰胺合成路线 （共 69 条）
反应条件
in N,N-dimethyl-formamide T=25°C; electroreduction; Rate constantEquilibrium constant;
参考文献
Maran, Flavio; Celadon, Dino; Severin, Maria Gabriella; Vianello, Elio
Journal of the American Chemical Society, 1991 , vol. 113, # 24 p. 9320 - 9329
反应条件
1: 29 percent / AlCl3 / xylene / 5 h / Heating 2: conc. HCl / 0.58 h View Scheme
参考文献
Chakraborty, D. P.; Mandal, Anchal Kanti; Roy, Swapan Kumar
Synthesis, 1981 , # 12 p. 977 - 979
反应条件
hydrogenchloride; sodium hydroxide T=95°C; 5 h; Yield given;
参考文献
Parry, Ronald J.; Mizusawa, A.E.; Chiu, I.C.; Naidu, M.V.; Ricciardone, M.
Journal of the American Chemical Society, 1985 , vol. 107, # 8 p. 2512 - 2521
反应条件
1: chlorosulfuric acid 2: aqueous ammonia View Scheme
参考文献
Adams; Long; Johanson
Journal of the American Chemical Society, 1939 , vol. 61, p. 2342,2344
反应条件
triethylamine in tetrahydrofuran
T=20°C; 19 h; Cooling with ice;
参考文献
SEMICONDUCTOR ENERGY LABORATORY CO., LTD.; INOUE, Hideko; NAKAGAWA, Tomoka; OHSAWA, Nobuharu; SEO, Satoshi; YAMADA, Yui
Patent: WO2011/52516 A1, 2011 ;
Location in patent: Page/Page column 104 ;
反应条件
oxygen; sodium hydroxide in water
T=40°C; 24 h; Green chemistry;
参考文献
Zhang, Leilei; Wang, Wentao; Wang, Aiqin; Cui, Yitao; Yang, Xiaofeng; Huang, Yanqiang; Liu, Xiaoyan; Liu, Wengang; Son, Jin-Young; Oji, Hiroshi; Zhang, Tao
Green Chemistry, 2013 , vol. 15, # 10 p. 2680 - 2684
反应条件
copper(l) iodide; water; caesium carbonate; potassium hydroxide; N-methyl-2-(methylamino)ethylamine
T=100°C; 15 h; Inert atmosphereSchlenk technique;
参考文献
Xiang, Shi-Kai; Zhang, Dong-Xue; Hu, Hao; Shi, Jiang-Ling; Liao, Li-Guo; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua; Yu, Wen-Hao
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 8 p. 1495 - 1499
反应条件
nickel in ethanol
T=90°C; 7 h;
参考文献
Parry, Ronald J.; Mizusawa, A.E.; Chiu, I.C.; Naidu, M.V.; Ricciardone, M.
Journal of the American Chemical Society, 1985 , vol. 107, # 8 p. 2512 - 2521
反应条件
aniline in tetrahydrofuran
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2011/101854 A1, 2011 ;
反应条件
2,4,6-trichloro-1,3,5-triazine; zinc(II) chloride in acetonitrile
Beckmann rearrangement; 1 h; Heating;
参考文献
Furuya, Yoshiro; Ishihara, Kazuaki; Yamamoto, Hisashi
Journal of the American Chemical Society, 2005 , vol. 127, # 32 p. 11240 - 11241
