2-甲基-N-苯基丙酰胺合成路线 （共 69 条）
反应条件
pivaloyl chloride in dichloromethane; N,N-dimethyl-formamide
T=20°C; Beckmann rearrangement; 8 h;
参考文献
Narahari, Srinivasa Reddy; Reguri, Buchi Reddy; Mukkanti
Tetrahedron Letters, 2011 , vol. 52, # 38 p. 4888 - 4891
反应条件
2,4,6-trichloro-1,3,5-triazine in N,N-dimethyl-formamide
T=20°C; Beckmann rearrangement; 12 h;
参考文献
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea
Journal of Organic Chemistry, 2002 , vol. 67, # 17 p. 6272 - 6274
反应条件
1-(2,4,6-triisopropyl-benzenesulfonyl)-1H-tetrazole in 1,2,3,4-tetrahydro-naphthalene; acetone
0.166667 h;
参考文献
Misharin; Chernov
Russian Journal of Bioorganic Chemistry, 1997 , vol. 23, # 8 p. 616 - 620
反应条件
cobalt
T=170°C; P=183877 Torr;
参考文献
Natta et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4496
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Pino; Paleari
Gazzetta Chimica Italiana, 1951 , vol. 81, p. 646,648
反应条件
trifluorormethanesulfonic acid; tris(4-methylphenyl)-phosphine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,2-dichloro-ethane
Beckmann rearrangement; 3 h; Heating;
参考文献
Arisawa, Mieko; Yamaguchi, Masahiko
Organic Letters, 2001 , vol. 3, # 2 p. 311 - 312
反应条件
hydroxylamine hydrochloride; trifluoroacetic acid
T=70°C; Beckmann Rearrangement; 16 h; Inert atmosphere;
参考文献
Arico, Fabio; Quartarone, Giuseppe; Rancan, Elia; Ronchin, Lucio; Tundo, Pietro; Vavasori, Andrea
Catalysis Communications, 2014 , vol. 49, p. 47 - 51
反应条件
potassium tert-butylate; water; oxygen in tetrahydrofuran
T=20°C; 0.166667 h;
参考文献
Kim, Bo Ram; Lee, Hyung-Geun; Kang, Seung-Beom; Sung, Gi Hyeon; Kim, Jeum-Jong; Park, Jong Keun; Lee, Sang-Gyeong; Yoon, Yong-Jin
Synthesis, 2012 , vol. 44, # 1 art. no. F77211SS, p. 42 - 50
反应条件
hydrogen
T=100°C; P=760.051 Torr; 24 h; Sealed tube;
参考文献
Li, Min; Hu, Lei; Cao, Xueqin; Hong, Haiyan; Lu, Jianmei; Gu, Hongwei
Chemistry - A European Journal, 2011 , vol. 17, # 9 p. 2763 - 2768
反应条件
triethylamine in benzene
0.25 h;
参考文献
Doszczak, Leszek; Rachon, Janusz
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1271 - 1279
反应条件
in dichloromethane
T=20°C; 6 h; Inert atmosphere;
参考文献
Hesp, Kevin D.; Bergman, Robert G.; Ellman, Jonathan A.
Journal of the American Chemical Society, 2011 , vol. 133, # 30 p. 11430 - 11433
