2-甲基-N-苯基丙酰胺合成路线 （共 69 条）
反应条件
bis(1,5-cyclooctadiene)nickel (0); sulfuric acid; tri-cyclo-hexyl-phosphine
1.) THF, -78 deg C -> r.t., 20 h; 2.) toluol, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hoberg, Heinz; Suemmermann, Klaus; Hernandez, Elisa; Ruppin, Christophe; Guhl, Dieter
Journal of Organometallic Chemistry, 1988 , vol. 344, p. C35 - C38
反应条件
n-butyllithium; iodine
Yield given. Multistep reaction;
参考文献
Keller, L.; Times-Marshall, K.; Behar, S.; Richards, K.
Tetrahedron Letters, 1989 , vol. 30, # 26 p. 3373 - 3376
反应条件
in acetonitrile
1 h; Ambient temperature; Yield given;
参考文献
Furukawa, M.; Hokama, N.; Okawara, T.
Synthesis, 1983 , # 1 p. 42 - 44
反应条件
1: isobutyryl 2-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl) sulfide in benzene
2 h; Heating;
2: aniline in benzene
cooling; Further stages.;
参考文献
Doszczak, Leszek; Rachon, Janusz
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1271 - 1279
反应条件
lithium diisopropyl amide
1. THF, -78 deg C, 1.5 h, 2. THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Endo, Yasuyuki; Hizatate, Shoji; Shudo, Koichi
Tetrahedron Letters, 1991 , vol. 32, # 24 p. 2803 - 2806
反应条件
bis(1,5-cyclooctadiene)nickel (0); sulfuric acid; diethylphosphinoethane
1.) THF, -20 deg C -> 70 deg C, 1 h; 2.) THF, 70 deg C, 40 h; Yield given. Multistep reaction;
参考文献
Hoberg, Heinz; Suemmermann, Klaus; Hernandez, Elisa; Ruppin, Christophe; Guhl, Dieter
Journal of Organometallic Chemistry, 1988 , vol. 344, p. C35 - C38
反应条件
tetra-n-butylammonium perchlorate
1.) CH3CN, electrolysis at -1.1 V, 2.) CH3CN, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Maran, Flavio; Fabrizio, Monica; D'Angeli, Ferruccio; Vianello, Elio
Tetrahedron, 1988 , vol. 44, # 8 p. 2351 - 2358
反应条件
lithium diisopropyl amide
1. THF, -78 deg C, 1.5 h, 2. THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Endo, Yasuyuki; Hizatate, Shoji; Shudo, Koichi
Tetrahedron Letters, 1991 , vol. 32, # 24 p. 2803 - 2806
反应条件
tetrabutylammomium bromide
electrochemical reduction at -1.4 V; Yield given. Yields of byproduct given;
参考文献
Maran, Flavio; Vianello, Elio; D'Angeli, Ferruccio; Cavicchioni, Giorgio; Vecchiati, Giorgio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 33 - 39
反应条件
lithium diisopropyl amide
multistep reaction, anionic <3,3>-sigmatropic rearrangement of N-phenyl-O-acylhydroxylamines, other N-phenyl-N-isobutyryl-O-acylhydroxylamines as educts; Product distribution;
参考文献
Endo, Yasuyuki; Hizatate, Shoji; Shudo, Koichi
Tetrahedron Letters, 1991 , vol. 32, # 24 p. 2803 - 2806
