3-苯基丙-2-烯-1-醇合成路线 (共 318 条)
参考文献
Shimizu, Masamichi; Kimura, Masanari; Tamaru, Yoshinao
Chemistry - A European Journal, 2005 , vol. 11, # 22 p. 6629 - 6642
反应条件
magnesium sulfate; 1,2-(p-MeOC6H4)2cyclobuten[=P(2,4,6-tri-t-BuPh)]2PdOTf in toluene T=20°C; 10 h;
参考文献
Yang, Shyh-Chyun; Hsu, Yi-Chun; Gan, Kim-Hong
Tetrahedron, 2006 , vol. 62, # 17 p. 3949 - 3958
反应条件
in dichloromethane T=20°C; 0.5 h;
参考文献
Lee, Eunsung; Yandulov, Dmitry V.
Journal of Fluorine Chemistry, 2009 , vol. 130, # 5 p. 474 - 483
反应条件
tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; titanium(IV) isopropylate in dichloromethane T=-15 - 0°C; Sharpless epoxidation;
参考文献
Chen, Jian; Lin, Guo-Qiang; Liu, Han-Quan
Tetrahedron Letters, 2004 , vol. 45, # 43 p. 8111 - 8113
反应条件
titanium(IV) isopropylate; tert.-butylhydroperoxide; (-)-(1S,3S)-1,2-bis(2-methoxyphenyl)ethane-1,2-diol in dichloromethane T=-20°C; 18 h;
参考文献
Yamamoto, Koji; Ando, Hiroyuki; Shuetake, Takashi; Chikamatsu, Hiroaki
Journal of the Chemical Society, Chemical Communications, 1989 , # 12 p. 754 - 756
反应条件
lt;N-(1,8-naphthalenedicarbonyl)-tert-Leu-lt;N-bis(1-naphthyl); vanadium triisopropoxide oxide in toluene T=0°C; 80 h; Title compound not separated from byproducts.;
参考文献
Hoshino; Yamamoto
Journal of the American Chemical Society, 2000 , vol. 122, # 42 p. 10452 - 10453
反应条件
tetrachloromethane; cross-linked polymer (containing 2.50 mmol of phosphine/g) 4 h; Heating;
参考文献
Chaudhari, Sachin S.; Akamanchi, Krishnacharya G.
Synlett, 1999 , # 11 p. 1763 - 1765
反应条件
1: trichloromonobromomethane With triphenylphosphine in dichloromethane T=20°C; Appel reaction; 0.666667 h; in air; 2: 3-phenyl-2-propen-1-ol (cinnamyl alcohol) in dichloromethane T=20°C; Appel reaction; in air;
参考文献
Newman, Stephen G.; Bryan, Christopher S.; Perez, Didier; Lautens, Mark
Synthesis, 2011 , # 2 art. no. Z27210SS, p. 342 - 346
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; trichloroisocyanuric acid in dichloromethane T=20°C; 0.0833333 h;
参考文献
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea
Organic Letters, 2001 , vol. 3, # 19 p. 3041 - 3043
反应条件
acetyl chloride in dichloromethane 1.) 0 deg C, 2.) room temperature, 1 h; Yields of byproduct given;
参考文献
Strazzolini, Paolo; Giumanini, Angelo G.; Verardo, Giancarlo
Tetrahedron, 1994 , vol. 50, # 1 p. 217 - 254