3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
copper; Cu(II) perchlorate; ethyl acetate 8 h; Yield given;
参考文献
Yasuda, Makoto; Somyo, Toshio; Baba, Akio
Angewandte Chemie - International Edition, 2006 , vol. 45, # 5 p. 793 - 796
反应条件
lithium chloride; bis-triphenylphosphine-palladium(II) chloride in diethylene glycol dimethyl ether T=120°C; 18 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 21 p. 2833 - 2836
反应条件
pyrrolidine; [PtCl2(η2:η2-cycloocta-1,5-diene)]; acetic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=60°C; 5 h; Inert atmosphereSchlenk techniqueMicrowave irradiation; SolventTemperatureTime; regioselective reaction;
参考文献
Shibuya, Ryozo; Lin, Lu; Nakahara, Yasuhito; Mashima, Kazushi; Ohshima, Takashi
Angewandte Chemie - International Edition, 2014 , vol. 53, # 17 p. 4377 - 4381
Angew. Chem., 2014 , vol. 126, # 17 p. 4466 - 4470,5
反应条件
triethylamine; zinc(II) chloride; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether T=85°C; 18 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 21 p. 2833 - 2836
反应条件
Pt(COD)Cl2; bis[2-(diphenylphosphino)phenyl] ether in 1,4-dioxane 12 h; Heating;
参考文献
Organic Letters, , vol. 9, # 17 p. 3371 - 3374
反应条件
1.1: manganese dioxide; NaBH4; 4A MS / CH2Cl2 / 17 h / Heating 1.2: 86 percent / MeOH / 0.67 h / 0 - 20 °C 2.1: 91 percent / NaH2PO4 / dioxane / 0.33 h / 60 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 43, # 41 p. 7337 - 7340
反应条件
α,α,α-trifluorotoluene; magnesium oxide T=83°C; 24 h; Title compound not separated from byproducts;
参考文献
Poon, Kevin W. C.; Dudley, Gregory B.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3923 - 3927
反应条件
osmium(VIII) oxide in water; tert-butyl alcohol T=20°C; 19 h; Inert atmosphere;
参考文献
Synthesis (Germany), , vol. 45, # 20 art. no. SS-2013-T0380-OP, p. 2875 - 2887
反应条件
tetrapropylammonium perruthennate in dichloromethane 0.5 h; Molecular sieveInert atmosphere;
参考文献
Synthesis (Germany), , vol. 45, # 20 art. no. SS-2013-T0380-OP, p. 2875 - 2887
反应条件
1: 4-methylbenzenesulfonic acid N-methylidene-hydrazide With sodium hydride in toluene; mineral oil T=0 - 20°C; 0.5 h; Inert atmosphere; 2: carbon monoxide; 3-phenyl-2-propen-1-ol (cinnamyl alcohol) With tris-(dibenzylideneacetone)dipalladium(0); Aliquat® 336; potassium carbonate in toluene; mineral oil T=60°C; P=760.051 Torr; 23 h;
参考文献
Zhang, Zhenhua; Liu, Yiyang; Ling, Lin; Li, Yuxue; Dong, Yian; Gong, Mingxing; Zhao, Xiaokun; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4330 - 4341
