3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
Schreiner's catalyst; 4-pyrrolidin-1-ylpyridine in octane 24 h; Reflux;
参考文献
Ishihara, Kazuaki; Niwa, Masatoshi; Kosugi, Yuji
Organic Letters, 2008 , vol. 10, # 11 p. 2187 - 2190
反应条件
2-methyl-5-methylpyridine; 4,5-dichloro-1,2,3-dithiazolium chloride in dichloromethane 1) -78 deg C, 2 h, 2) to room temperature, 12 h;
参考文献
Folmer; Weinreb
Tetrahedron Letters, 1993 , vol. 34, # 17 p. 2737 - 2740
反应条件
tetra-(n-butyl)ammonium iodide; triethylamine in N,N-dimethyl-formamide 5 h; Heating;
参考文献
Soltani Rad, Mohammad Navid; Behrouz, Somayeh; Faghihi, Mohammad Ali; Khalafi-Nezhad, Ali
Tetrahedron Letters, 2008 , vol. 49, # 7 p. 1115 - 1120
反应条件
1: With N-hydroxyphthalimide resin; amidosulfamic acid in dichloromethane T=20°C; Mitsunobu reaction; 24 h; 2: With methylamine in methanol; chloroform T=20°C; 2 h;
参考文献
Maillard, Ludovic T.; Benohoud, Meryem; Durand, Philippe; Badet, Bernard
Journal of Organic Chemistry, 2005 , vol. 70, # 16 p. 6303 - 6312
反应条件
1: 2,2,6-trimethyl-4H-1,3-dioxin-4-one; 3-phenyl-2-propen-1-ol (cinnamyl alcohol) in tetrahydrofuran Heating; 2: 4-Acetylaminobenzenesulfonyl Azide in acetonitrile T=20°C; 3: With lithium hydroxide
参考文献
Bioorganic and medicinal chemistry letters, , vol. 12, # 24 p. 3561 - 3563
反应条件
1: K2CO3 / CH2Cl2 / 20 °C 2: DBU; N,N'-ditosylhydrazine / tetrahydrofuran / 0 °C View Scheme
参考文献
Organic Letters, , vol. 9, # 16 p. 3195 - 3197
反应条件
N,N-dimethyl-aniline; triethylamine 1.) CH2Cl2, 0 deg C, 15 min, 2.) CH2Cl2, from 0 deg C to RT, 3.75 h; Yield given. Multistep reaction;
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 11 p. 2259 - 2269
反应条件
propylamine; 4 A molecular sieve; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in tetrahydrofuran T=50°C; 24 h; Title compound not separated from byproducts.;
参考文献
Yamashita, Yasuhiro; Gopalarathnam, Apsara; Hartwig, John F.
Journal of the American Chemical Society, 2007 , vol. 129, # 24 p. 7508 - 7509
反应条件
tricyclo[3.3.1.13,7 ]-decane-1-carboxylic acid; triphenylphosphine; bis(acetylacetonato) palladium in water 0.5 h; Heating;
参考文献
Yang, Shyh-Chyun; Hsu, Yi-Chun; Gan, Kim-Hong
Tetrahedron, 2006 , vol. 62, # 17 p. 3949 - 3958
反应条件
(+)-tartrate derived dioxaborolane; diethylzinc Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 49 p. 9181 - 9184
