3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
palladium diacetate in acetonitrile
T=25°C; 24 h; Yield givenYields of byproduct given;
参考文献
Matoba, Kazutaka; Motofusa, Shin-Ichi; Sik Cho, Chan; Ohe, Kouichi; Uemura, Sakae
Journal of Organometallic Chemistry, 1999 , vol. 574, # 1 p. 3 - 10
反应条件
N-bromosuccinmide; triphenylphosphine in tetrahydrofuran
T=-18 - 80°C; 1 h;
参考文献
Froyen, Paul; Juvvik, Paul
Tetrahedron Letters, 1995 , vol. 36, # 52 p. 9555 - 9558
反应条件
1: Br2 / CH2Cl2 / 0.33 h / 0 °C
2: NaN3 / dimethylsulfoxide / 24 h / 20 °C
3: aq. NaOH / dimethylsulfoxide / 92 h / 0 °C
4: 55 percent / MnO2 / CHCl3 / 16 h / 20 °C
View Scheme
参考文献
Alajarin, Mateo; Orenes, Raul-Angel; Vidal, Angel; Pastor, Aurelia
Synthesis, 2003 , # 1 p. 49 - 52
反应条件
manganese(IV) oxide; sodium cyanide; acetic acid
T=20°C; 168 h;
参考文献
Foot, Jonathan S.; Kanno, Hisashi; Giblin, Gerard M. P.; Taylor, Richard J. K.
Synthesis, 2003 , # 7 p. 1055 - 1064
反应条件
tetra-n-butylammonium acetate; palladium diacetate
T=80°C; Heck arylation; 0.5 h;
参考文献
Calo, Vincenzo; Nacci, Angelo; Monopoli, Antonio; Ferola, Valentina
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2596 - 2601
反应条件
tetra-n-butylammonium acetate; palladium diacetate
T=80°C; Heck arylation; 0.5 h;
参考文献
Calo, Vincenzo; Nacci, Angelo; Monopoli, Antonio; Ferola, Valentina
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2596 - 2601
反应条件
oxygen; TEAB; Co(TPP) in ethylene glycol dimethyl ether; isopropyl alcohol
192 h; Ambient temperature;
参考文献
Okamoto, Tadashi; Oka, Shinzaburo
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1589 - 1594
反应条件
bis(η3-allyl-μ-chloropalladium(II)); C32H25NP2 in 1,4-dioxane
T=80°C; 4 h; Inert atmosphere;
参考文献
Ghosh, Raju; Sarkar, Amitabha
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8508 - 8512
反应条件
Erwaermen des Reaktionsprodukts mit HBr in Eisessig auf 100grad;
参考文献
Foeldi
Chemische Berichte, 1930 , vol. 63, p. 2262
反应条件
1: Sharpless epoxidation
2: NaIO4, RuCl3
View Scheme
参考文献
Legters, J.; Thijs, L.; Zwanenburg, B.
Tetrahedron Letters, 1989 , vol. 30, # 36 p. 4881 - 4884
