3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
phosphoric acid in water; toluene
T=25°C; P=760.051 Torr; pH=3.4; 24 h; IrradiationInert atmosphereSealed tube; Overall yield = 89 percent; chemoselective reaction;
参考文献
Liu, Zijun; Caner, Joaquim; Kudo, Akihiko; Naka, Hiroshi; Saito, Susumu
Chemistry - A European Journal, 2013 , vol. 19, # 29 p. 9452 - 9456
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in toluene
T=200°C;
参考文献
Kondo, Teruyuki; Yang, Sungbong; Huh, Keun-Tae; Kobayashi, Masanobu; Kotachi, Shinji; Watanabe, Yoshihisa
Chemistry Letters, 1991 , p. 1275 - 1278
反应条件
hydrogenchloride; manganese(IV) oxide; 4 A molecular sieve in diethyl ether; toluene
T=105°C; 18 h;
参考文献
Wilfred, Cecilia D.; Taylor, Richard J. K.
Synlett, 2004 , # 9 p. 1628 - 1630
反应条件
platinum (II) chloride in dichloromethane
T=60°C; 20 h;
参考文献
Lester, Roy P.; Dunsford, Jay J.; Camp, Jason E.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 43 p. 7472 - 7476
反应条件
1: 100 percent / NaH / diethyl ether / -10 °C
2: 100 percent / xylene / Heating
View Scheme
参考文献
Knezevic, Anamarija; Landek, Goran; Dokli, Irena; Vinkovic, Vladimir
Tetrahedron Asymmetry, 2011 , vol. 22, # 9 p. 936 - 941
反应条件
palladium diacetate; tributylphosphine; diethylzinc in hexane; toluene
T=20°C; 6 h;
参考文献
Kimura, Masanari; Shimizu, Masamichi; Tanaka, Shuji; Tamaru, Yoshinao
Tetrahedron, 2005 , vol. 61, # 15 p. 3709 - 3718
反应条件
in toluene
T=80°C; 1 h;
参考文献
Lin, Ken-Ching; Shen, Yi-Ling; Rao, N. S. Kameswara; Liao, Chun-Chen
Journal of Organic Chemistry, 2002 , vol. 67, # 23 p. 8157 - 8165
反应条件
manganese(IV) oxide; triazolium salt; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene
T=20°C;
参考文献
Maki, Brooks E.; Chan, Audrey; Phillips, Eric M.; Scheidt, Karl A.
Organic Letters, 2007 , vol. 9, # 2 p. 371 - 374
反应条件
titanium tetraethoxide; triethylamine; zinc(II) chloride; bis-triphenylphosphine-palladium(II) chloride in diethylene glycol dimethyl ether
T=120°C; 18 h;
参考文献
Itoh, Kenji; Hamaguchi, Naoki; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 21 p. 2833 - 2836
反应条件
triphenyl phosphite; [Ir(μ-Cl)(1,5-cyclooctadiene)]2; sodium hydride
1.) THF, 2.) THF, reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Takeuchi, Ryo; Kashio, Mikihiro
Journal of the American Chemical Society, 1998 , vol. 120, # 34 p. 8647 - 8655
