3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
With polymer-supported dicyanoketene acetal; water in acetonitrile T=20°C; Hydrolysis; 24 h;
参考文献
Tanaka, Nobuyuki; Masaki, Yukio Synlett, 1999 , # 12 p. 1960 - 1962
反应条件
With ZBHNMP in tetrahydrofuran T=20°C; 1.08333 h;
参考文献
Tajbakhsh; Lakouraj; Mohanazadeh; Ahmadi-Nejhad Synthetic Communications, 2003 , vol. 33, # 2 p. 229 - 236
反应条件
With diisopropoxytitanium(III) tetrahydroborate in dichloromethane T=-20°C; 0.133333 h;
参考文献
Ravikumar; Chandrasekaran, Srinivasan Journal of Organic Chemistry, 1996 , vol. 61, # 3 p. 826 - 830
反应条件
Multi-step reaction with 3 steps 1: MCPBA / CH2Cl2 / 0 deg C, 1.5 h, then RT, 24 h2: 1.) NaOH / 1.) H2O, 70 deg C; 2.) H2O, 70 deg C, 2.5 h3: 61 percent / pyridine / 2 h / -10 °C
参考文献
Melloni; Della Torre; Lazzari; et al. Tetrahedron, 1985 , vol. 41, # 7 p. 1393 - 1399
反应条件
Multi-step reaction with 4 steps 1: MCPBA / CH2Cl2 / 0 deg C, 1.5 h, then RT, 24 h2: 1.) NaOH / 1.) H2O, 70 deg C; 2.) H2O, 70 deg C, 2.5 h3: 61 percent / pyridine / 2 h / -10 °C4: 84 percent / Et3N / CH2Cl2 / 0.5 h / 0 - 5 °C
参考文献
Melloni; Della Torre; Lazzari; et al. Tetrahedron, 1985 , vol. 41, # 7 p. 1393 - 1399
反应条件
With H3[PW12O40]; poly(acrylamide) based ammonium salt; dihydrogen peroxide T=20°C; 30 h;
参考文献
Yamada, Yoichi M.A.; Tabata, Hidetsugu; Ichinohe, Masato; Takahashi, Hideyo; Ikegami, Shiro Tetrahedron, 2004 , vol. 60, # 18 p. 4087 - 4096
反应条件
Multi-step reaction with 2 steps 1: pyridine2: R(a)-2,2'-binaphthyl-bis-((R)-1-phenylethyl)phosphoramidite / [Ir(cod)Cl]2 / tetrahydrofuran / 10 h / 20 °C
参考文献
Ohmura, Toshimichi; Hartwig, John F. Journal of the American Chemical Society, 2002 , vol. 124, # 51 p. 15164 - 15165
反应条件
With N-chloro-succinimide; [{Cp*IrCl2}]2 in tetrahydrofuran; water T=20°C; 23 h;
参考文献
Ahlsten, Nanna; Gomez, Antonio Bermejo; Martin-Matute, Belen Angewandte Chemie - International Edition, 2013 , vol. 52, # 24 p. 6273 - 6276Angew. Chem., 2013 , vol. 125, # 24 p. 6393 - 6396,4
反应条件
With sodium azide; triphenylphosphine in dichloromethane; N,N-dimethyl-formamide T=90°C; Substitution; Mitsunobu reaction; Staudinger reaction; 4 h;
参考文献
Vidya Sagar Reddy; Venkat Rao; Subramanyam; Iyengar Synthetic Communications, 2000 , vol. 30, # 12 p. 2233 - 2237
反应条件
Multi-step reaction with 3 steps 1: NaH / diethyl ether / 0 - 20 °C2: xylene / 14 h / Heating3: 82 percent / 6N NaOH / ethanol / 40 h / 20 °C
参考文献
Boucard, Valerie; Sauriat-Dorizon, Helene; Guibe, Francois Tetrahedron, 2002 , vol. 58, # 36 p. 7275 - 7290
