3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
tert.-butylhydroperoxide; cis-[RuII(6,6'-Cl2bpy)2(OH)2](CF3SO3)2 in acetone T=20°C; Oxidation; 48 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 23 p. 7996 - 8000
参考文献
Zetzsche; Zala
Helvetica Chimica Acta, 1926 , vol. 9, p. 289
反应条件
1.1: triethylamine / dichloromethane / 15 h / 20 °C / |Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / |Inert atmosphere 2.2: 15 h / 0 - 20 °C / |Inert atmosphere 3.1: sec.-butyllithium / tetrahydrofuran / -78 °C / |Inert atmosphere View Scheme
参考文献
Fournier, Anne M.; Nichols, Christopher J.; Vincent, Mark A.; Hillier, Ian H.; Clayden, Jonathan
Chemistry - A European Journal, 2012 , vol. 18, # 51 p. 16478 - 16490
反应条件
1: pyridine 2: hydrotalcite-supported Au nanoparticles / toluene / 3 h / 80 °C / Inert atmosphere View Scheme
参考文献
Noujima, Akifumi; Mitsudome, Takato; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Chemical Communications, 2012 , vol. 48, # 53 p. 6723 - 6725
反应条件
1: pyridine 2: hydrogen / toluene / 12 h / 80 °C / 760.05 Torr View Scheme
参考文献
Noujima, Akifumi; Mitsudome, Takato; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Chemical Communications, 2012 , vol. 48, # 53 p. 6723 - 6725
反应条件
1: pyridine 2: hydrogen / toluene / 12 h / 80 °C / 760.05 Torr View Scheme
参考文献
Noujima, Akifumi; Mitsudome, Takato; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Chemical Communications, 2012 , vol. 48, # 53 p. 6723 - 6725
反应条件
α,α,α-trifluorotoluene; magnesium oxide T=83°C; 24 h; Title compound not separated from byproducts;
参考文献
Poon, Kevin W. C.; Dudley, Gregory B.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3923 - 3927
反应条件
bis(cyclopentadienyl)zirconium dihydride in isopropyl alcohol T=130°C; 8 h;
参考文献
Nakano, Tatsuya; Umano, Shigetoshi; Kino, Yoshio; Ishii, Yasutaka; Ogawa, Masaya
Journal of Organic Chemistry, 1988 , vol. 53, # 16 p. 3752 - 3757
反应条件
3-methyl-5-deaza-10-oxaflavin; toluene-4-sulfonic acid in 1,4-dioxane 1 h; Heatingother 3-methyl-5-deaza-10-oxaflavins; other alcohols; Product distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 2 p. 307 - 311
反应条件
hydrogenchloride; aluminum isopropoxide in ethyl acetate; benzene
